外消旋2-羟基-4,6-二甲氧基-苯甲酸1-甲基-5-氧代-9-癸烯-1-基酯合成路线 （共 5 条）
反应条件
triphenylphosphine; diethylazodicarboxylate in diethyl ether T=20°C; Esterification; Mitsunobu reaction; 3 h;
参考文献
Furstner; Thiel; Kindler; Bartkowska
Journal of Organic Chemistry, 2000 , vol. 65, # 23 p. 7990 - 7995
反应条件
1: 77 percent / diethyl ether; tetrahydrofuran / -78 - 20 °C 2: 64 percent / PPh3; DEAD / diethyl ether / 3 h / 20 °C View Scheme
参考文献
Furstner; Thiel; Kindler; Bartkowska
Journal of Organic Chemistry, 2000 , vol. 65, # 23 p. 7990 - 7995
反应条件
1: 77 percent / diethyl ether; tetrahydrofuran / -78 - 20 °C 2: 64 percent / PPh3; DEAD / diethyl ether / 3 h / 20 °C View Scheme
参考文献
Furstner; Thiel; Kindler; Bartkowska
Journal of Organic Chemistry, 2000 , vol. 65, # 23 p. 7990 - 7995
反应条件
in pyridine; dichloromethane T=0°C; trifluoromethylsulfonylation; 3 h;
参考文献
Furstner; Thiel; Kindler; Bartkowska
Journal of Organic Chemistry, 2000 , vol. 65, # 23 p. 7990 - 7995
反应条件
1: 92 percent / CH2Cl2; pyridine / 3 h / 0 °C 2: 93 percent / LiCl; Et3N; PdCl2(PPh3)2 / dimethylformamide / 20 h / 90 °C / 41254.1 Torr View Scheme
参考文献
Furstner; Thiel; Kindler; Bartkowska
Journal of Organic Chemistry, 2000 , vol. 65, # 23 p. 7990 - 7995
