2-N-Cbz-氨基-环己酮合成路线 （共 8 条）
反应条件
oxalyl dichloride; triethylamine in dimethyl sulfoxide
参考文献
Bersot, Ross; Humphries, Paul
Patent: US2013/303524 A1, 2013 ;
Location in patent: Paragraph 0423-0424 ;
反应条件
1: aq. NaHCO3 / methanol 2: (ClCO)2, Et3N / dimethylsulfoxide View Scheme
参考文献
Bersot, Ross; Humphries, Paul
Patent: US2013/303524 A1, 2013 ;
反应条件
1: NH4OH / methanol / Heating 2: aq. NaHCO3 / methanol 3: (ClCO)2, Et3N / dimethylsulfoxide View Scheme
参考文献
Angle, Steven R.; Arnaiz, Damian O.
Tetrahedron Letters, 1989 , vol. 30, # 5 p. 515 - 518
反应条件
1: triethylamine / tetrahydrofuran / 0 - 20 °C 2: Jone's reagent / 2.5 h / 20 °C View Scheme
参考文献
Bersot, Ross; Humphries, Paul
Patent: US2013/303524 A1, 2013 ;
参考文献
Lessard,J. et al.
Tetrahedron Letters, 1970 , p. 4887 - 4890
反应条件
1: CrCl2, NaOMe 2: aq. AcOH View Scheme
参考文献
Lessard,J. et al.
Tetrahedron Letters, 1970 , p. 4887 - 4890
反应条件
1: CrCl2, NaOMe 2: aq. AcOH View Scheme
参考文献
Lessard,J. et al.
Tetrahedron Letters, 1970 , p. 4887 - 4890
反应条件
(i) CrCl2, (ii) NaOMe, MeOH; Multistep reaction;
参考文献
Driguez,H. et al.
Canadian Journal of Chemistry, 1978 , vol. 56, p. 119 - 130
