反应条件
1.1: magnesium / tetrahydrofuran / 3 h / |Inert atmosphere; |Reflux 1.2: -78 - 20 °C / |Inert atmosphere 1.3: -78 - 20 °C / |Inert atmosphere 2.1: (SPY-5-31)-dichloro-(κ2(C,O)-(2-isopropyloxybenzylidene))(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)ruthenium / toluene / 24 h / 60 °C / |Inert atmosphere 3.1: hydrogen; 5 palladium on charcoal / methanol / 48 h View Scheme
参考文献
Carr, Damien J.; Kudavalli, Jaya Satyanarayana; Dunne, Katherine S.; Mueller-Bunz, Helge; Gilheany, Declan G.
Journal of Organic Chemistry, 2013 , vol. 78, # 20 p. 10500 - 10505
