2-(3-氯苯基)-1-(3-吡啶基)-1-乙酮合成路线 （共 5 条）
参考文献
Ciba-Geigy Corporation
Patent: US3940486 A1, 1976 ;
反应条件
hydrogenchloride in tetrahydrofuran; water; isopropyl alcohol 2 h; Ambient temperature; Yield given;
参考文献
Journet, Michel; Cai, Dongwei; Larsen, Robert D.; Reider, Paul J.
Tetrahedron Letters, 1998 , vol. 39, # 13 p. 1717 - 1720
反应条件
1: 86 percent / propan-2-ol / 4 h / Ambient temperature 2: anh. Cs2CO3 / tetrahydrofuran; propan-2-ol / 16 h / Ambient temperature 3: 3N HCl / H2O; tetrahydrofuran; propan-2-ol / 2 h / Ambient temperature View Scheme
参考文献
Journet, Michel; Cai, Dongwei; Larsen, Robert D.; Reider, Paul J.
Tetrahedron Letters, 1998 , vol. 39, # 13 p. 1717 - 1720
反应条件
1: anh. Cs2CO3 / tetrahydrofuran; propan-2-ol / 16 h / Ambient temperature 2: 3N HCl / H2O; tetrahydrofuran; propan-2-ol / 2 h / Ambient temperature View Scheme
参考文献
Journet, Michel; Cai, Dongwei; Larsen, Robert D.; Reider, Paul J.
Tetrahedron Letters, 1998 , vol. 39, # 13 p. 1717 - 1720
反应条件
sodium hydroxide; hydrazine in ethylene glycol T=140 - 145°C; Wolf-Kishner reduction; 6 - 10 h; Product distribution / selectivity;
参考文献
MOREPEN LABORATORIES LIMITED
Patent: WO2006/6184 A2, 2006 ;
Location in patent: Page/Page column 13-14 ;
