1-溴-2-(2-(2-(2-溴乙氧基)乙氧基)乙氧基)乙烷合成路线 （共 20 条）
反应条件
1: 50 percent / tetrabutylammonium iodide, sodium hydroxide (50 percent) / toluene; H2O / 9 h / Heating 2: 47 percent / lithium aluminum hydride / tetrahydrofuran / 20 h / Heating View Scheme
参考文献
Lukyanenko, Nikolai G.; Basok, Stepan S.; Filonova, Lyubov K.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 3141 - 3148
反应条件
in N,N-dimethyl-formamide
参考文献
Bogatskii, A.V.; Luk'yanenko, N. G.; Kirichenko, T. I.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, p. 1124 - 1129
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 6 p. 1301 - 1307
反应条件
1: 18 percent / KOH 2: 90.1 percent Spectr. / Me4NOH / dimethylsulfoxide; H2O / 25 °C View Scheme
参考文献
Illuminati, Gabriello; Mandolini, Luigi; Masci, Bernardo
Journal of the American Chemical Society, 1981 , vol. 103, # 14 p. 4142 - 4145
反应条件
sodium hydroxide; tetra-(n-butyl)ammonium iodide in toluene 16 h; Heating;
参考文献
Bogaschenko, Tatyana; Basok, Stepan; Kulygina, Catherine; Lyapunov, Alexander; Lukyanenko, Nikolay
Synthesis, 2002 , # 15 p. 2266 - 2270
反应条件
sodium iodide in acetone
72 h; Ambient temperature;
参考文献
Black, David St. C.; Horsham, Mark A.; Rose, Michael
Tetrahedron, 1995 , vol. 51, # 16 p. 4819 - 4828
反应条件
1: 82 percent / tetrabutylammonium iodide, sodium hydroxide (50 percent) / toluene; H2O / 9 h / Heating
2: 45 percent / lithium aluminum hydride / tetrahydrofuran / 20 h / Heating
View Scheme
参考文献
Lukyanenko, Nikolai G.; Basok, Stepan S.; Filonova, Lyubov K.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 3141 - 3148
反应条件
1: 66 percent / dimethylformamide
2: 48 percent / 1) hydrazine hydrate, 2) 6N aq. HCl / Heating
3: 34 percent / ethanol
View Scheme
参考文献
Bogatskii, A.V.; Luk'yanenko, N. G.; Kirichenko, T. I.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, p. 1124 - 1129
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 6 p. 1301 - 1307
参考文献
Shtamburg, V. G.; Skobelev, O. L.; Grinev, V. M.; Dmitrienko, A. D.; Pleshkova, A. P.; Pritykin, L. M.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 5 p. 609 - 612
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 5 p. 660 - 664
反应条件
1: 86 percent / tetrabutylammonium iodide, sodium hydroxide (50 percent) / toluene; H2O / 9 h / Heating
2: 68 percent / lithium aluminum hydride / tetrahydrofuran / 20 h / Heating
View Scheme
参考文献
Lukyanenko, Nikolai G.; Basok, Stepan S.; Filonova, Lyubov K.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 3141 - 3148
反应条件
caesium carbonate in N,N-dimethyl-formamide
T=50°C;
参考文献
Buter, Jan; Kellogg, Richard M.
Journal of the Chemical Society, Chemical Communications, 1980 , # 11 p. 466 - 467
