9-苯基-10-三甲基硅烷基菲合成路线 (共 2 条)
反应条件
1: 2,2'-dibromobiphenyl With n-butyllithium in tetrahydrofuran T=-78°C; 1 h; 2: With anhydrous chromium(III) chloride in tetrahydrofuran T=20°C; 1 h; 3: 1-trimethylsilyl-2-phenylacetylene in tetrahydrofuran T=50°C; 24 h;
参考文献
Kanno, Ken-Ichiro; Liu, Yuanhong; Iesato, Atsushi; Nakajima, Kiyohiko; Takahashi, Tamotsu
Organic Letters, 2005 , vol. 7, # 24 p. 5453 - 5456
反应条件
iodine cloride in dichloromethane
参考文献
Campo; Larock
Organic letters, 2000 , vol. 2, # 23 p. 3675 - 3677