(6aR,10aR)-6,6,9-三甲基-3-丙基-6A,7,8,10A-四氢-6H-苯并[c]苯并吡喃-1-醇合成路线 (共 2 条)
反应条件
potassium tert-butylate; water in tert-butyl alcohol T=65°C; 4.5 h;
参考文献
MALLINCKRODT INC.
Patent: WO2009/99868 A1, 2009 ;
Location in patent: Page/Page column 28-29 ;
反应条件
1: With magnesium sulfate in dichloromethane T=20°C; 0.166667 h; 2: With boron trifluoride diethyl etherate in dichloromethane T=3 - 12°C;
参考文献
MALLINCKRODT INC.
Patent: WO2009/99868 A1, 2009 ;
Location in patent: Page/Page column 28 ;