in solid 135°C; monitored by TLC on Silufol plates (silica gel layer);
参考文献
Kukishkin, V. Yu.; Moiseev, A. I.; Sidorov, E. O.
Journal of General Chemistry USSR (English Translation), 1989 , vol. 59, p. 1750 - 1759
Zhurnal Obshchei Khimii, 1989 , vol. 59, p. 1958 - 1966
in further solvent(s) heating of trans-Pt(Py)(Et2SO)Cl2 in diethylsulfoxide in flask equipped with a refluxer; cooling; addn. of H2O or Et2O; pptn., filtration, monitoring by NMR;
参考文献
De Vekki
Russian Journal of Inorganic Chemistry, 2008 , vol. 53, # 8 p. 1238 - 1241
in further solvent(s) dissolving of trans-Pt(Py)(Et2SO)Cl2 in diethylsulfoxide in flask equipped with a refluxer; heating at 100°C for 9 h; cooling; addn. of H2O or Et2O; pptn., filtration, monitoring by NMR;
参考文献
De Vekki
Russian Journal of Inorganic Chemistry, 2008 , vol. 53, # 8 p. 1238 - 1241
in further solvent(s) dissolving of cis-Pt(Py)2Cl2 in diethylsulfoxide in flask equipped with a refluxer; heating at 80°C for 14 h; cooling; addn. of H2O or Et2O; pptn., filtration, monitoring by NMR;
参考文献
De Vekki
Russian Journal of Inorganic Chemistry, 2008 , vol. 53, # 8 p. 1238 - 1241
in further solvent(s) dissolving of trans-Pt(Py)2Cl2 in diethylsulfoxide in flask equipped with a refluxer; heating at 70-100°C for 16 h; cooling; addn. of H2O or Et2O; pptn., filtration, monitoring by NMR;
参考文献
De Vekki
Russian Journal of Inorganic Chemistry, 2008 , vol. 53, # 8 p. 1238 - 1241
in further solvent(s) heating of Pt(Py)4Cl2 in diethylsulfoxide in flask equipped with a refluxer; cooling; addn. of H2O or Et2O; pptn., filtration, monitoring by NMR; as mixt. of isomers;
参考文献
De Vekki
Russian Journal of Inorganic Chemistry, 2008 , vol. 53, # 8 p. 1238 - 1241
in further solvent(s) dissolving of cis-Pt(Py)2Cl2 in diethylsulfoxide in flask equipped with a refluxer; heating at 80°C for 14 h; further exposure of reaction mixt.; cooling; addn. of H2O or Et2O; pptn., filtration, monitoring by NMR; as mixt. of cis- and trans-isomers;
参考文献
De Vekki
Russian Journal of Inorganic Chemistry, 2008 , vol. 53, # 8 p. 1238 - 1241