3-醛基吲哚-7-甲酸甲酯合成路线 (共 1 条)
反应条件
1: N,N-dimethyl-formamide With trichlorophosphate in 1,2-dichloro-ethane T=5°C; 2: 1H-Indole-7-carboxylic acid,methyl ester in 1,2-dichloro-ethane T=5 - 50°C; 2.5 h; 3: With water; sodium carbonate in dichloromethane T=20°C; 0.5 h;
参考文献
Abbott GmbH and Co. KG
Patent: US7049312 B1, 2006 ;
Location in patent: Page/Page column 112 ;
US 7049312 B1