4-甲基-1,10-邻二氮杂菲合成路线 （共 12 条）
反应条件
sulfuric acid; sodium iodide T=140 - 145°C; 6 h;
参考文献
Lutun, Stephane; Guichard, Eric; Hasiak, Bruno; Couturier, Daniel
Synthetic Communications, 1999 , vol. 29, # 2 p. 175 - 180
反应条件
sulfuric acid; sodium iodide T=110°C; 5 h;
参考文献
Belser, Peter; Bernhard, Stefan; Guerig, Urs
Tetrahedron, 1996 , vol. 52, # 8 p. 2937 - 2944
反应条件
1: 50 percent / HNO3, conc.H2SO4 / 1.) 0 deg C, 2 h, 2.) room temperature, 12 h 2: 98 percent / NaBH4 / Pd/C / methanol / 0.5 h 3: 66 percent / NaI, conc.H2SO4 / 6 h / 140 - 145 °C View Scheme
参考文献
Synthetic Communications, , vol. 29, # 2 p. 175 - 180
反应条件
1: 98 percent / NaBH4 / Pd/C / methanol / 0.5 h 2: 66 percent / NaI, conc.H2SO4 / 6 h / 140 - 145 °C View Scheme
参考文献
Synthetic Communications, , vol. 29, # 2 p. 175 - 180
反应条件
sodium hydroxide 1.) acetonitrile, 75 deg C; Yield given. Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 104, # 5 p. 1319 - 1330
反应条件
sodium hydroxide 1.) acetonitrile, 20 deg C; Yield given. Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 104, # 5 p. 1319 - 1330
反应条件
sodium hydroxide 1.) acetonitrile, 22 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 104, # 5 p. 1319 - 1330
反应条件
sodium hydroxide 1.) acetonitrile, 70 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 104, # 5 p. 1319 - 1330
反应条件
tris(phenanthroline)iron(III) tris(hexafluorophosphate) in acetonitrile T=0°C; competition with BrCCL3, other complexes; Rate constant;
参考文献
Journal of the American Chemical Society, , vol. 104, # 5 p. 1319 - 1330
反应条件
sodium hydroxide 1.) acetonitrile, 22 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 104, # 5 p. 1319 - 1330
