3-(4-氯苯基)异噁唑合成路线 (共 16 条)
反应条件
1: Br2 / CH2Cl2 / 0.33 h / 0 °C 2: NaN3 / dimethylsulfoxide / 24 h / 20 °C 3: aq. NaOH / dimethylsulfoxide / 92 h / 0 °C 4: 7 percent / MnO2 / CHCl3 / 5 h / 20 °C View Scheme
参考文献
Synthesis, , # 1 p. 49 - 52
反应条件
triethylamine in chloroform
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 7, p. 2051 - 2055
Zhurnal Organicheskoi Khimii, , vol. 7, p. 1979 - 1984
反应条件
1: With triethylamine in trichloroethane, 1,1,2- 0.5 h; Heating; 2: With sodium hydroxide 0.5 h; Heating;
参考文献
Magnetic Resonance in Chemistry, , vol. 44, # 9 p. 851 - 855
反应条件
1: thiophenol With lithium diisopropyl amide in tetrahydrofuran; hexane T=0°C; 0.166667 h; Inert atmosphere; 2: 3-(p-chlorophenyl)isoxazole in tetrahydrofuran; hexane T=-98°C; 1.01667 h; Inert atmosphere;
参考文献
Synthesis, , # 18 p. 3195 - 3203
反应条件
1: thiophenol With lithium diisopropyl amide in tetrahydrofuran; hexane T=0°C; 0.166667 h; Inert atmosphere; 2: 3-(p-chlorophenyl)isoxazole in tetrahydrofuran; hexane T=-98°C; 1.01667 h; Inert atmosphere;
参考文献
Synthesis, , # 18 p. 3195 - 3203
反应条件
molybdenum hexacarbonate in benzene 20 h; Heating; Product distributionMechanism;
参考文献
Kobayashi, Tomoshige; Nitta, Makoto
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 1 p. 152 - 157