反应条件
in neat (no solvent) byproducts: 9,9-dichloro-9-silafluorene, 10,10-Cl2-9-oxa-10-sila-9,10-dihydrophenanthren; pyrolysis at 660, 680, 710, 730, 750°C in quartz flow reactor; sepn. by fractional distn.; fraction with b.p. 185-205°C contains mixt. of HCl2Si(OSiCl2)2Cl and Cl3Si(OSiCl2)2Cl;
参考文献
Journal of General Chemistry USSR (English Translation), , vol. 62, p. 1502 - 1509
Zhurnal Obshchei Khimii, , vol. 62, p. 1828 - 1837