3,3-二甲基-1-苯基-1-丁酮合成路线 （共 36 条）
反应条件
2,4,6-trimethyl-pyridine; 2,2'-azo-bisisobutyronitrile in benzene 3 h; Heating;
参考文献
Cai, Yudong; Roberts, Brian P.; Tocher, Derek A.; Barnett, Sarah A.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 17 p. 2517 - 2529
反应条件
cerium(III) chloride; lithium perchlorate in tetrahydrofuran electrolysis;
参考文献
Fry, Albert J.; Susla, Marko; Weltz, Michael
Journal of Organic Chemistry, 1987 , vol. 52, # 12 p. 2496 - 2498
参考文献
Pettersson, Ingrid; Berg, Ulf
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 1365 - 1376
反应条件
18-crown-6 ether; potassium tert-butylate 1.) Me2SO, 2.) irradiation, 6 h; Yield given. Multistep reaction;
参考文献
Russell, Glen A.; Khanna, Rajive K.
Tetrahedron, 1985 , vol. 41, # 19 p. 4133 - 4146
反应条件
hydrogenchloride; n-butyllithium; N,N,N',N,-tetramethylethylenediamine 1) THF, 0 deg C, 1 h, r.t., 20.5 h, 2) MeOH, heating, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Kanemasa, Shui; Tanaka, Junji; Nagahama, Hideki; Tsuge, Otohiko
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 11 p. 3385 - 3386
反应条件
sodium hydroxide; sodium dihydrogenphosphate; dihydrogen peroxide 1.) 150 deg C, 4 h, 2.) 0 deg C, 2 h, pentane; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Binnewirtz, Ralf-Juergen; Klingenberger, Helmut; Welte, Rainer; Paetzold, Peter
Chemische Berichte, 1983 , vol. 116, # 4 p. 1271 - 1284
反应条件
sodium hydroxide; sodium dihydrogenphosphate; dihydrogen peroxide 1.) 100 deg C, 4 h, 2.) 0 deg C, 2 h, pentane; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Binnewirtz, Ralf-Juergen; Klingenberger, Helmut; Welte, Rainer; Paetzold, Peter
Chemische Berichte, 1983 , vol. 116, # 4 p. 1271 - 1284
反应条件
thionyl chloride; silica gel in dichloromethane 3 h; various reaction times and adsorbent; Product distribution;
参考文献
Kropp, Paul J.; Crawford, Scott D.
Journal of Organic Chemistry, 1994 , vol. 59, # 11 p. 3102 - 3112
反应条件
silica gel; phosphorus tribromide in dichloromethane 0.3 h; various reaction times and adsorbent; Product distribution;
参考文献
Kropp, Paul J.; Crawford, Scott D.
Journal of Organic Chemistry, 1994 , vol. 59, # 11 p. 3102 - 3112
反应条件
silica gel; phosphorus(III) iodide in dichloromethane 0.3 h; various reaction times and adsorbent; Product distribution;
参考文献
Kropp, Paul J.; Crawford, Scott D.
Journal of Organic Chemistry, 1994 , vol. 59, # 11 p. 3102 - 3112
