Α-(对甲苯磺酰)苯乙酮合成路线 (共 66 条)
反应条件
Oxonereg;; aluminium trichloride Oxidation; 0.5 h; Heating;
参考文献
Hajipour, A. R.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1997 , vol. 36, # 11 p. 1069 - 1070
反应条件
N-benzyl-N,N,N-triethylammonium chloride in acetonitrile T=20°C; Acylation; 1.5 h;
参考文献
Ramaiah; Dubey; Ramanatham; Grossert; Hooper
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1999 , vol. 38, # 3 p. 297 - 301
反应条件
indium in water T=0°C; 4 h;
参考文献
Wang, Lei; Zhang, Yongmin
Journal of Chemical Research - Part S, 1998 , # 9 p. 588 - 589
反应条件
T=30°C; 5 h; Ionic liquid;
参考文献
Kumar, Anil; Muthyala, Manoj Kumar
Tetrahedron Letters, 2011 , vol. 52, # 41 p. 5368 - 5370
反应条件
perchloric acid in 1,4-dioxane T=50°C; 4 h;
参考文献
Journal of Organic Chemistry, , vol. 48, # 18 p. 3077 - 3084
反应条件
silver nitrate in tetrahydrofuran; water T=20°C; 24 h; Inert atmosphere; Reagent/catalystTimeSolvent;
参考文献
Chinese Chemical Letters, , vol. 23, # 10 p. 1115 - 1118,4
反应条件
pyridine; oxygen in 1,2-dichloro-ethane T=20 - 45°C; P=760.051 Torr; 4.08 h; Schlenk technique;
参考文献
Lu, Qingquan; Zhang, Jian; Zhao, Ganglu; Qi, Yue; Wang, Huamin; Lei, Aiwen
Journal of the American Chemical Society, 2013 , vol. 135, # 31 p. 11481 - 11484
反应条件
trifluoroacetic acid in tetrahydrofuran T=50°C; 5 h;
参考文献
Qian, Hao; Huang, Xian
Synthesis, 2006 , # 12 p. 1934 - 1936
反应条件
1: p-toluenesulfinic acid sodium salt With hydrogenchloride in water T=22°C; 0.0333333 h; 2: phenylacetylene With 2,6-dimethylpyridine in water T=22°C; 1.33333 h; 3: p-toluenesulfinic acid sodium salt With 2,6-dimethylpyridine; hydrogenchloride in water T=22°C; 6 h; Reagent/catalystConcentrationTemperatureTime;
参考文献
Handa, Sachin; Fennewald, James C.; Lipshutz, Bruce H.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 13 p. 3432 - 3435
Angew. Chem., 2014 , vol. 126, # 13 p. 3500 - 3503,4
反应条件
fac-Ir(ppy)3 in dichloromethane T=20°C; 8 h; Inert atmosphereIrradiation; SolventReagent/catalyst;
参考文献
Jiang, Heng; Cheng, Yuanzheng; Zhang, Yan; Yu, Shouyun
European Journal of Organic Chemistry, 2013 , # 24 p. 5485 - 5492