Α-(对甲苯磺酰)苯乙酮合成路线 （共 66 条）
反应条件
in dimethyl sulfoxide; acetonitrile T=20°C; 1 h;
参考文献
Samakkanad, Natthapol; Katrun, Praewpan; Techajaroonjit, Thanachart; Hlekhlai, Sornsiri; Pohmakotr, Manat; Reutrakul, Vichai; Jaipetch, Thaworn; Soorukram, Darunee; Kuhakarn, Chutima
Synthesis (Germany), 2012 , vol. 44, # 11 art. no. SS-2012-N0148-OP, p. 1693 - 1699
反应条件
titanium(IV) isopropylate; diethyl (2R,3R)-tartrate; 5-(1-hydroperoxyethyl)-3-ethoxycarbonyl-2-isopropylfuran in dichloromethane T=-25°C; 17 h; other racemic β-keto sulfoxides; var. hydroperoxides; var. time and temp.; Product distribution;
参考文献
Tetrahedron Asymmetry, , vol. 9, # 15 p. 2619 - 2625
反应条件
2: 30percent H2O2, acetic acid View Scheme
参考文献
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, , vol. 28, # 2 p. 154 - 158
反应条件
2: 30percent H2O2, acetic acid View Scheme
参考文献
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, , vol. 28, # 2 p. 154 - 158
反应条件
1: acetone / 48 h / 30 °C 2: 5 h / 30 °C / Ionic liquid View Scheme
参考文献
Tetrahedron Letters, , vol. 52, # 41 p. 5368 - 5370
反应条件
boron trifluoride diethyl etherate; triphenylbismuth(V) difluoride 1.) CH2Cl2, room temperature, 10 h, 2.) DMF, room temperature, 24 h; Yield given. Multistep reaction;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 13 p. 1739 - 1748
参考文献
Journal of Organic Chemistry, , vol. 40, # 26 p. 3857 - 3862
反应条件
1: K2CO3 / acetonitrile / 20 °C 2: 96 percent / KCl; hydrogen peroxide / acetone / 6 h / 20 °C 3: 99 percent / aq. NaOH / 0.5 h / 20 °C View Scheme
参考文献
Suryakiran; Prabhakar; Srikanth Reddy; Chinni Mahesh; Rajesh; Venkateswarlu
Tetrahedron Letters, 2007 , vol. 48, # 5 p. 877 - 881
反应条件
[NiI2(PPh3)]; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=80°C; Kumada Cross-Coupling; Inert atmosphere;
参考文献
Wu, Ji-Cheng; Gong, Lu-Bing; Xia, Yuanzhi; Song, Ren-Jie; Xie, Ye-Xiang; Li, Jin-Heng
Angewandte Chemie - International Edition, 2012 , vol. 51, # 39 p. 9909 - 9913
反应条件
[NiI2(PPh3)]; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=80°C; Kumada Cross-Coupling; Inert atmosphere;
参考文献
Wu, Ji-Cheng; Gong, Lu-Bing; Xia, Yuanzhi; Song, Ren-Jie; Xie, Ye-Xiang; Li, Jin-Heng
Angewandte Chemie - International Edition, 2012 , vol. 51, # 39 p. 9909 - 9913
