Α-(对甲苯磺酰)苯乙酮合成路线 （共 66 条）
反应条件
[NiI2(PPh3)]; tri-cyclo-hexyl-phosphine in tetrahydrofuran
T=80°C; Kumada Cross-Coupling; Inert atmosphere;
参考文献
Wu, Ji-Cheng; Gong, Lu-Bing; Xia, Yuanzhi; Song, Ren-Jie; Xie, Ye-Xiang; Li, Jin-Heng
Angewandte Chemie - International Edition, 2012 , vol. 51, # 39 p. 9909 - 9913
反应条件
sodium ethanolate in ethanol
T=0°C;
参考文献
Jong, Kwan Bin; Jae, Sang Lee; Kim, Kyongtae
Organic Letters, 2004 , vol. 6, # 23 p. 4297 - 4300
反应条件
acetic anhydride; zinc(II) chloride
T=120 - 140°C;
参考文献
Neplyuev,V.M. et al.
Journal of Organic Chemistry USSR (English Translation), 1977 , vol. 13, p. 1341 - 1345
Zhurnal Organicheskoi Khimii, 1977 , vol. 13, # 7 p. 1456 - 1461
反应条件
1: 96 percent / KI; hydrogen peroxide / acetone / 4 h / 20 °C
2: 98 percent / aq. NaOH / 0.5 h / 20 °C
View Scheme
参考文献
Suryakiran; Srikanth Reddy; Suresh; Lakshman; Venkateswarlu
Tetrahedron Letters, 2006 , vol. 47, # 26 p. 4319 - 4323
反应条件
1: 99 percent / KBr; hydrogen peroxide / acetone / 2 h / 20 °C
2: 99 percent / aq. NaOH / 0.5 h / 20 °C
View Scheme
参考文献
Suryakiran; Prabhakar; Srikanth Reddy; Chinni Mahesh; Rajesh; Venkateswarlu
Tetrahedron Letters, 2007 , vol. 48, # 5 p. 877 - 881
反应条件
N-benzyl-trimethylammonium hydroxide
参考文献
Truce; Wellisch
Journal of the American Chemical Society, 1952 , vol. 74, p. 2881
