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1: 1.) aq. NaOH / 1.) toluene, 1 h, 2.) 25 deg C 2: 8.3 g / dimethylformamide / 25 °C 3: 85 percent / dimethylformamide / 132 h / 35 °C View Scheme

sodium hydroxide 1.) toluene, 1 h, 2.) 25 deg C; Multistep reaction;