2-氯-4,6-二甲氧基-1,3,5-三嗪合成路线 （共 40 条）
反应条件
in acetonitrile-D3 1 h;
参考文献
Kunishima, Munetaka; Ujigawa, Takae; Nagaoka, Yoshie; Kawachi, Chiho; Hioki, Kazuhito; Shiro, Motoo
Chemistry - A European Journal, 2012 , vol. 18, # 49 p. 15856 - 15867
反应条件
palladium on activated charcoal; diethyl ether Hydrogenation.unter Zusatz von Triaethylamin;
参考文献
Flament et al.
Helvetica Chimica Acta, 1959 , vol. 42, p. 485 - 489
反应条件
triethylamine in isopropyl alcohol T=20°C; Eschenmoser Methylenation; 0.25 h;
参考文献
Tetrahedron Letters, , vol. 54, # 13 p. 1758 - 1760
参考文献
Davies, Alwyn G.; Sutcliffe, Roger
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 1512 - 1519
反应条件
4-methyl-morpholine in N,N-dimethyl-formamide
参考文献
The Trustees of Princeton University
Patent: US6066732 A1, 2000 ;
反应条件
4-methyl-morpholine; benzoic acid; citric acid in dichloromethane; acetonitrile
参考文献
ROHM AND HAAS COMPANY
Patent: EP982292 A2, 2000 ;
反应条件
in N,N-dimethyl-formamide T=25°C; 24 h; Inert atmosphere;
参考文献
Melzig, Laurin; Metzger, Albrecht; Knochel, Paul
Chemistry - A European Journal, 2011 , vol. 17, # 10 p. 2948 - 2956
反应条件
potassium hydroxide in tetrahydrofuran T=20°C;
参考文献
Li, Xiao-Jian; Zhang, Jin-Ling; Geng, Yu; Jin, Zhong
Journal of Organic Chemistry, 2013 , vol. 78, # 10 p. 5078 - 5084
反应条件
sodium azide in ethanol T=30 - 40°C; Yield given;
参考文献
Azev, Yu. A.; Gusel'nikova, O. L.; Klyuev, N. A.; Shorshnev, S. V.; Rusinov, V. L.; Chupakhin, O. N.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 10 p. 1418 - 1424
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 10 p. 1566 - 1572
反应条件
1: 90 percent / sodium carbonate, hydroxylamine hydrochloride / methanol; H2O / 0.17 h / Ambient temperature 2: MnO2 / CHCl3 / 1 h / Ambient temperature View Scheme
参考文献
Sedova. V. F.; Shkurko, O. P.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1993 , vol. 29, # 5 p. 593 - 597
Khimiya Geterotsiklicheskikh Soedinenii, 1993 , # 5 p. 694 - 699
