3,3-二甲基-2,4-戊二酮合成路线 (共 46 条)
反应条件
potassium carbonate in dimethyl sulfoxide 72 h; Ambient temperature;
参考文献
Beck, Karin; Huenig, Siegfried
Chemische Berichte, 1987 , vol. 120, p. 477 - 484
反应条件
potassium carbonate in acetone 30 h; Heating;
参考文献
Itoh, Osamu; Iwakoshi, Naoki; Saitoh, Toshihide; Katano, Hiroaki; Fujisawa, Yoshiki; et al.
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 1 p. 177 - 181
反应条件
hydrogen; palladium on activated charcoal in methanol 1 h; Ambient temperature;
参考文献
Chemische Berichte, , vol. 113, # 11 p. 3621 - 3628
反应条件
zinc(II) chloride T=110°C;
参考文献
Journal of the American Chemical Society, , vol. 75, p. 626
反应条件
ozone; ethenetetracarbonitrile in methyl acetate T=-60°C;
参考文献
Chemische Berichte, , vol. 97, p. 2681 - 2688
反应条件
potassium carbonate in tetrahydrofuran; dimethyl sulfoxide T=10 - 20°C; 72 h;
参考文献
Medicinal Chemistry Research, , vol. 22, # 3 p. 1147 - 1162
反应条件
sulfuric acid T=-10°C;
参考文献
Zhurnal Obshchei Khimii, , vol. 11, p. 1119
Chem.Abstr., , p. 3735
反应条件
1: aq. HCl / methanol 2: NaOMe / bis-(2-methoxy-ethyl) ether / 159 °C 3: TCNE, O3 / methyl acetate / -60 °C View Scheme
参考文献
Chemische Berichte, , vol. 97, p. 2681 - 2688
反应条件
1: NaOMe / bis-(2-methoxy-ethyl) ether / 159 °C 2: TCNE, O3 / methyl acetate / -60 °C View Scheme
参考文献
Chemische Berichte, , vol. 97, p. 2681 - 2688
参考文献
Journal of the American Chemical Society, , vol. 53, p. 2301,2307