4-氨基-3-硝基二苯甲酮合成路线 （共 16 条）
反应条件
ammonium hydroxide in formamide T=120°C; P=3000.2 - 3750.3 Torr; 6 h;
参考文献
Niclas, Hans-Joachim; Bohle, Matthias; Rick, Jens-Detlev; Zeuner, Frank; Zoelch, Lothar
Zeitschrift fuer Chemie (Stuttgart, Germany), 1985 , vol. 25, # 4 p. 137 - 138
反应条件
sodium hydroxide in methanol Hydrolysis; Heating;
参考文献
Organic Preparations and Procedures International, , vol. 23, # 5 p. 627 - 632
反应条件
potassium tert-butylate; N,N-tetramethylene-thiocarbamoyl-sulphenamide in N,N-dimethyl-formamide T=20°C; 0.333333 h;
参考文献
Journal of Organic Chemistry, , vol. 63, # 15 p. 4878 - 4888
反应条件
sodium hydroxide in methanol Hydrolysis; 3 h; Heating;
参考文献
Ayyangar, N. R.; Lahoti, R. J.; Daniel, Thomas
Organic Preparations and Procedures International, 1991 , vol. 23, # 5 p. 627 - 632
反应条件
zinc T=140 - 142°C; Friedel-Crafts acylation; 0.00833333 h; microwave irradiation;
参考文献
Paul, Satya; Nanda, Puja; Gupta, Rajive; Loupy, Andre
Synthesis, 2003 , # 18 p. 2877 - 2881
反应条件
1: 95 percent / fuming HNO3 2: aq. NaOH / methanol / Heating View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 23, # 5 p. 627 - 632
反应条件
1: 98 percent / AlCl3 / 1,2-dichloro-ethane / 5 h / 0 - 5 °C 2: 96 percent / fuming HNO3 / 0.75 h / 0 - 25 °C 3: 94 percent / aq. NaOH / methanol / 3 h / Heating View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 23, # 5 p. 627 - 632
反应条件
1: 96 percent / fuming HNO3 / 0.75 h / 0 - 25 °C 2: 94 percent / aq. NaOH / methanol / 3 h / Heating View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 23, # 5 p. 627 - 632
反应条件
1: 98 percent / AlCl3 / 1,2-dichloro-ethane / 5 h / 0 - 5 °C 2: 96 percent / fuming HNO3 / 0.75 h / 0 - 25 °C 3: 94 percent / aq. NaOH / methanol / 3 h / Heating View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 23, # 5 p. 627 - 632
反应条件
ammonia T=130°C; im Druckrohr;
参考文献
Chemische Berichte, , vol. 24, p. 3768
