2-[(4-氯苯基)氨基]萘-1,4-二酮合成路线 （共 10 条）
反应条件
in neat (no solvent) T=100°C; P=750.075 Torr; 0.05 h; Microwave irradiation;
参考文献
Devi Bala, Balasubramanian; Muthusaravanan, Sivasubramanian; Perumal, Subbu
Tetrahedron Letters, 2013 , vol. 54, # 29 p. 3735 - 3739
反应条件
copper (II) acetate monohydrate; acetic acid T=60 - 70°C; 0.5 h; Under air;
参考文献
Lisboa, Cinthia Da S.; Santos, Vanessa G.; Vaz, Boniek G.; De Lucas, Nanci C.; Eberlin, Marcos N.; Garden, Simon J.
Journal of Organic Chemistry, 2011 , vol. 76, # 13 p. 5264 - 5273
反应条件
MgCl2*6H2O; toluene-4-sulfonic acid in methanol 7 h; Reflux;
参考文献
Francisco, Acacio I.; Vargas, Maria D.; Carneiro, J. Walkimar de M.; Lanznaster, Mauricio; Torres, Jose C.; Camara, Celso A.; Pinto, Angelo C.
Journal of Molecular Structure, 2008 , vol. 891, # 1-3 p. 228 - 232
反应条件
in pyridine T=130 - 140°C; 4 h;
参考文献
Agarwal, Nand L.; Schaefer, Wolfram
Journal of Organic Chemistry, 1980 , vol. 45, # 25 p. 5139 - 5143
反应条件
1: 1) 1,2,3-trichloropropane / 1) 110 deg C, 0.5 h; 2) 2.5 h, heating 2: 2 percent / pyridine / 4 h / 130 - 140 °C View Scheme
参考文献
Agarwal, Nand L.; Schaefer, Wolfram
Journal of Organic Chemistry, 1980 , vol. 45, # 25 p. 5139 - 5143
反应条件
1: 1) 1,2,3-trichloropropane / 1) 110 deg C, 0.5 h; 2) 2.5 h, heating 2: 2 percent / pyridine / 4 h / 130 - 140 °C View Scheme
参考文献
Agarwal, Nand L.; Schaefer, Wolfram
Journal of Organic Chemistry, 1980 , vol. 45, # 25 p. 5139 - 5143
反应条件
in tetrahydrofuran 0 deg C, 1 h, RT, 1 h, 55 deg C, 0.5 h;
参考文献
Matsuo, Koji; Shiraki, Ryuji; Okubo, Masao
Journal of Physical Organic Chemistry, 1994 , vol. 7, # 10 p. 567 - 577
反应条件
perchloric acid 1) pyridine, 110-130 deg C, 5 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Agarwal, Nand L.; Schaefer, Wolfram
Journal of Organic Chemistry, 1980 , vol. 45, # 25 p. 5139 - 5143
反应条件
perchloric acid 1) 110-130 deg C, 5 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Agarwal, Nand L.; Schaefer, Wolfram
Journal of Organic Chemistry, 1980 , vol. 45, # 25 p. 5139 - 5143
反应条件
pivaloyl chloride in benzene
T=20°C; Chlorination;
参考文献
Litvin, B. L.; Gubrii, Z. V.; Shermolovich, Yu. G.; Novikov, V. P.
Russian Journal of Organic Chemistry, 1999 , vol. 35, # 3 p. 377 - 383
Zhurnal Organicheskoi Khimii, 1999 , vol. 35, # 3 p. 401 - 407
