1-甲氧基-1-(三甲基甲硅氧基)-2-甲基-1-丙烯合成路线 (共 133 条)
反应条件
1: 2-methylpropanoic acid methyl ester With n-butyllithium; diisopropylamine in tetrahydrofuran; hexane 1 h; 2: chloro-trimethyl-silane in tetrahydrofuran; hexane 1 h;
参考文献
Paquette, Leo A.; Parker, Gregory D.; Tei, Takahiro; Dong, Shuzhi
Journal of Organic Chemistry, 2007 , vol. 72, # 19 p. 7124 - 7134
反应条件
2,6-di-tert-butyl-4-methyl-phenol; Rhodium trichloride in tetrahydrofuran T=40 - 50°C; other methacrylates;
参考文献
Revis, Anthony; Hilty, Terrence K.
Journal of Organic Chemistry, 1990 , vol. 55, # 9 p. 2972 - 2973
反应条件
triethylamine 144 h; Ambient temperature;
参考文献
Oesterle, Thomas; Simchen, Gerhard
Liebigs Annalen der Chemie, 1987 , p. 687 - 692
反应条件
sodium in octane T=105°C; 1 h; other molten alkali metals, other temperature; Product distribution;
参考文献
Schulz, William J.; Speier, John L.
Synthesis, 1989 , # 3 p. 163 - 166
反应条件
sodium 40 h; Heating;
参考文献
Schulz, William J.; Speier, John L.
Synthesis, 1989 , # 3 p. 163 - 166
反应条件
Rhodium trichloride Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 28, # 41 p. 4809 - 4812
参考文献
Journal of the Chemical Society [Section] D: Chemical Communications, , p. 136 - 137
反应条件
Ti-β titanium silicate in dichloromethane T=39.84°C; 5 h; regioselective reaction;
参考文献
Sasidharan, Manickam; Bhaumik, Asim
Journal of Molecular Catalysis A: Chemical, 2011 , vol. 346, # 1-2 p. 87 - 93
反应条件
triethylamine hydrofluoric acid in dichloromethane 1.) 30 min, RT, 2.) 5-10 h, RT;
参考文献
Rubottom, George M.; Gruber, John M.; Marrero, Roberto; Juve, Henrik D.; Kim, Wan Chong
Journal of Organic Chemistry, 1983 , vol. 48, # 25 p. 4940 - 4944
反应条件
InI3; phenyl silane in dichloromethane T=20°C; 1 h;
参考文献
Inamoto, Yoshihiro; Nishimoto, Yoshihiro; Yasuda, Makoto; Baba, Akio
Chemistry Letters, 2013 , vol. 42, # 12 p. 1551 - 1553