1-甲氧基-1-(三甲基甲硅氧基)-2-甲基-1-丙烯合成路线 (共 133 条)
反应条件
P[2,4,6-(OMe)3C6H2]3 in N,N-dimethyl-formamide
T=20°C; 1 h;
参考文献
Matsukawa, Satoru; Obu, Kayoko
Chemistry Letters, 2004 , vol. 33, # 12 p. 1626 - 1627
反应条件
tris(pentafluorophenyl)-borane
1.) toluene, a) -78 deg C, 4 h, b) RT, 12 h, 2.) toluene. ether, RT, 1 d; Yield given. Multistep reaction;
参考文献
Ishihara, Kazuaki; Hanaki, Naoyuki; Funahashi, Miyuki; Miyata, Mayumi; Yamamoto, Hisashi
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 6 p. 1721 - 1730
反应条件
Yield given. Multistep reaction;
参考文献
Colvin; McGarry; Nugent
Tetrahedron, 1988 , vol. 44, # 13 p. 4157 - 4172
反应条件
Yield given. Multistep reaction;
参考文献
Colvin, Ernest W.; McGarry, Daniel G.
Journal of the Chemical Society, Chemical Communications, 1985 , # 9 p. 539 - 540
反应条件
bis(.pi.-allylpalladium chloride); N,N,N',N,-tetramethylethylenediamine; thallous acetate in dichloromethane
3 h; Ambient temperaturealso with CH3-CH=CH-CH2Br; other allyl complex; other ligand; var. reaction time; Product distributionMechanism;
参考文献
Formica, Mauro; Musco, Alfredo; Pontellini, Roberto; Linn, Klaus; Mealli, Carlo
Journal of Organometallic Chemistry, 1993 , vol. 448, # 1.2 p. C6 - C9
反应条件
lithium perchlorate in diethyl ether
0.5 h; Ambient temperature;
参考文献
Ipaktschi, Junes; Heydari, Akbar
Chemische Berichte, 1992 , vol. 125, # 6 p. 1513 - 1516
反应条件
zinc chloride on alumina
T=20°C; Solid phase reaction; Mukaiyama aldol reaction; 2 h; sonication;
参考文献
Ranu, Brindaban C.; Saha, Manika; Bhar, Sanjay
Synthetic Communications, 1997 , vol. 27, # 17 p. 3065 - 3077
反应条件
1,3-bis(1-adamantyl)imidazolin-2-ylidene in tetrahydrofuran
T=23°C; 20 h; Inert atmosphere;
参考文献
Song, Jinhua J.; Tan, Zhulin; Reeves, Jonathan T.; Fandrick, Daniel R.; Yee, Nathan K.; Senanayake, Chris H.
Organic Letters, 2008 , vol. 10, # 5 p. 877 - 880
反应条件
ZnF2; tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine in DMF (N,N-dimethyl-formamide)
T=80°C; 18 h;
参考文献
AMR Technology, Inc.
Patent: US2006/63808 A1, 2006 ;
Location in patent: Page/Page column 11; 14 ;
反应条件
zinc(II) chloride in nitromethane
T=-25°C; 4 h;
参考文献
Reetz, Manfred T.; Schwellnus, Konrad; Huebner, Friedhelm; Massa, Werner; Schmidt, Roland E.
Chemische Berichte, 1983 , vol. 116, # 11 p. 3708 - 3724