1-甲氧基-1-(三甲基甲硅氧基)-2-甲基-1-丙烯合成路线 （共 133 条）
反应条件
zinc(II) chloride in nitromethane
T=-25°C; 4 h;
参考文献
Reetz, Manfred T.; Schwellnus, Konrad; Huebner, Friedhelm; Massa, Werner; Schmidt, Roland E.
Chemische Berichte, 1983 , vol. 116, # 11 p. 3708 - 3724
反应条件
zinc(II) chloride in nitromethane
T=-25°C; 4 h; further solvent: CH2Cl2 at r.t.;
参考文献
Reetz, Manfred T.; Schwellnus, Konrad; Huebner, Friedhelm; Massa, Werner; Schmidt, Roland E.
Chemische Berichte, 1983 , vol. 116, # 11 p. 3708 - 3724
反应条件
zinc(II) chloride in nitromethane
T=-25°C; 4 h;
参考文献
Reetz, Manfred T.; Schwellnus, Konrad; Huebner, Friedhelm; Massa, Werner; Schmidt, Roland E.
Chemische Berichte, 1983 , vol. 116, # 11 p. 3708 - 3724
反应条件
zinc(II) chloride in nitromethane
T=-25°C; 4 h;
参考文献
Reetz, Manfred T.; Schwellnus, Konrad; Huebner, Friedhelm; Massa, Werner; Schmidt, Roland E.
Chemische Berichte, 1983 , vol. 116, # 11 p. 3708 - 3724
反应条件
titanium tetrachloride in dichloromethane
T=-70 - 20°C; 2 h;
参考文献
Shono, Tatsuya; Tsubata, Kenji; Okinaga, Nobuyuki
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1056 - 1059
反应条件
1: 71 percent / TiCl4 / CH2Cl2 / 2 h / -70 - 20 °C
2: 66 percent / 25percent HBr / acetic acid / Ambient temperature
View Scheme
参考文献
Shono, Tatsuya; Tsubata, Kenji; Okinaga, Nobuyuki
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1056 - 1059
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane
5 h; Ambient temperature;
参考文献
Ikeda; Achiwa; Sekiya
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 5 p. 1179 - 1184
反应条件
trimethylsilyl trifluoromethanesulfonate in acetonitrile
T=30°C; 18 h;
参考文献
Ikeda, Kiyoshi; Achiwa, Kazuo; Sekiya, Minoru
Tetrahedron Letters, 1983 , vol. 24, # 43 p. 4707 - 4710
反应条件
trimethylsilyl trifluoromethanesulfonate in acetonitrile
T=30 - 35°C; 18 h;
参考文献
Ikeda; Achiwa; Sekiya
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 5 p. 1179 - 1184
反应条件
zinc dibromide in dichloromethane
T=20°C; 3 h;
参考文献
Alexander, Rikki P.; Paterson, Ian
Tetrahedron Letters, 1983 , vol. 24, # 52 p. 5911 - 5914
