1-甲氧基-1-(三甲基甲硅氧基)-2-甲基-1-丙烯合成路线 (共 133 条)
反应条件
lithium perchlorate in diethyl ether 0.5 h; Ambient temperatureother 1,4-quinones;
参考文献
Chemische Berichte, , vol. 125, # 6 p. 1513 - 1516
反应条件
SmI2(THF)2 in dichloromethane 0.5 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Hydrio, Jerome; Van De Weghe, Pierre; Collin, Jacqueline
Synthesis, 1997 , # 1 p. 68 - 72
反应条件
lithium perchlorate in diethyl ether 0.5 h; Ambient temperature;
参考文献
Ipaktschi, Junes; Heydari, Akbar
Chemische Berichte, 1992 , vol. 125, # 6 p. 1513 - 1516
反应条件
1: 1.) tris(dimethylamino)sulfonium difluorotrimethylsiliconate; 2.) 1 N HCl / 1.) pyridine, THF, -10 deg C to RT, 3.5 h; 2.) pyridine, THF, 5 min 2: 86 percent / DDQ / benzene / 18 h / Heating View Scheme
参考文献
RajanBabu, T. V.; Reddy, G. S.; Fukunaga, Tadamichi
Journal of the American Chemical Society, 1985 , vol. 107, # 19 p. 5473 - 5483
反应条件
1: With 2,3,4,5,6,6-hexachloro-2,4-cyclohexadienone in dichloromethane T=20°C; 2: With water in dichloromethane T=20°C; 0.5 h;
参考文献
Duan, Xin-Hua; Mayr, Herbert
Organic Letters, 2010 , vol. 12, # 10 p. 2238 - 2241
反应条件
dimethylphenylsilane; tris(pentafluorophenyl)-borane in dichloromethane T=20°C; Mukaiyama reaction; 2 h;
参考文献
Organic Letters, , vol. 14, # 4 p. 1168 - 1171
反应条件
InI3; phenyl silane in dichloromethane T=20°C; 1 h;
参考文献
Inamoto, Yoshihiro; Nishimoto, Yoshihiro; Yasuda, Makoto; Baba, Akio
Chemistry Letters, 2013 , vol. 42, # 12 p. 1551 - 1553
反应条件
InI3; dimethylmono-chlorosilane in dichloromethane T=20°C; 1 h; Reagent/catalyst;
参考文献
Inamoto, Yoshihiro; Nishimoto, Yoshihiro; Yasuda, Makoto; Baba, Akio
Chemistry Letters, 2013 , vol. 42, # 12 p. 1551 - 1553
反应条件
InI3; phenyl silane in dichloromethane T=20°C; 1 h;
参考文献
Inamoto, Yoshihiro; Nishimoto, Yoshihiro; Yasuda, Makoto; Baba, Akio
Chemistry Letters, 2013 , vol. 42, # 12 p. 1551 - 1553
反应条件
pyrene in acetonitrile 1 h; Irradiation;
参考文献
Tetrahedron Letters, , vol. 36, # 41 p. 7463 - 7466