1-甲氧基-1-(三甲基甲硅氧基)-2-甲基-1-丙烯合成路线 （共 133 条）
反应条件
ZnF2; tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium(0) in N,N-dimethyl-formamide T=80°C; 12 h;
参考文献
Hama, Takuo; Liu, Xiaoxiang; Culkin, Darcy A.; Hartwig, John F.
Journal of the American Chemical Society, 2003 , vol. 125, # 37 p. 11176 - 11177
反应条件
TiCl2(OPri)2; diisobutylaluminium hydride 1.) CH2Cl2, toluene, -78 deg C, 2 h, 2.) CH2Cl2, -78 deg C, 3 h; Yield given. Multistep reaction;
参考文献
Kiyooka; Suzuki; Shirouchi; Kaneko; Tanimori
Tetrahedron Letters, 1993 , vol. 34, # 36 p. 5729 - 5732
反应条件
TiCl2(OPri)2; diisobutylaluminium hydride 1.) CH2Cl2, toluene, -78 deg C, 2 h, 2.) CH2Cl2, -78 deg C, 3 h; Yield given. Multistep reaction;
参考文献
Kiyooka; Suzuki; Shirouchi; Kaneko; Tanimori
Tetrahedron Letters, 1993 , vol. 34, # 36 p. 5729 - 5732
反应条件
InI3; phenyl silane in dichloromethane T=20°C; 1 h; diastereoselective reaction;
参考文献
Inamoto, Yoshihiro; Nishimoto, Yoshihiro; Yasuda, Makoto; Baba, Akio
Chemistry Letters, 2013 , vol. 42, # 12 p. 1551 - 1553
反应条件
lithium hydroxide hydrate in N,N-dimethyl-formamide T=0 - 5°C; Mukaiyama-Michael reaction; Inert atmosphere;
参考文献
Tamagaki, Hiroaki; Nawate, Yuuya; Nagase, Ryohei; Tanabe, Yoo
Chemical Communications, 2010 , vol. 46, # 32 p. 5930 - 5932
反应条件
Ph3C+ClO4- in dichloromethane T=-78°C;
参考文献
Kobayashi, Shu; Mukaiyama, Teruaki
Chemistry Letters, 1987 , p. 1183 - 1186
反应条件
aluminum cation-exchanged montmorillonite in dichloromethane T=-10°C; 1 h;
参考文献
Kawai, Motomitsu; Onaka, Makoto; Izumi, Yusuke
Journal of the Chemical Society, Chemical Communications, 1987 , # 15 p. 1203 - 1204
反应条件
1: [(1-methoxy-2-methyl-1-propenyl)oxy]trimethylsilane; dicarbonyl(η5-cyclopentadienyl)[(1,2-η)propene]iron(II) tetrafluoroborate in dichloromethane T=0 - 20°C; 16 h; 2: methanol; carbon monoxide With ammonium cerium(IV) nitrate T=-78 - 20°C;
参考文献
Dulich, Felix; Mueller, Karl-Heinz; Ofial, Armin R.; Mayr, Herbert
Helvetica Chimica Acta, 2005 , vol. 88, # 7 p. 1754 - 1768
反应条件
1: 52 percent / aluminum ion-exchanged montmorillonite / CH2Cl2 / 1 h / -10 °C 2: 1M HCl / Ambient temperature View Scheme
参考文献
Kawai, Motomitsu; Onaka, Makoto; Izumi, Yusuke
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 2157 - 2164
反应条件
titanium tetrachloride 1.) CH2Cl2, 0.5 h, -80 deg C; Yield given. Multistep reaction;
参考文献
Rousseau, Gerard; Blanco, Luis
Tetrahedron Letters, 1985 , vol. 26, # 35 p. 4191 - 4194
