1-甲氧基-1-(三甲基甲硅氧基)-2-甲基-1-丙烯合成路线 (共 133 条)
反应条件
water; indium(III) chloride Mukaiyama aldol reaction; 24 h;
参考文献
Chan, Kok-Ping; Ling, Yvonne Hui; Loh, Teck-Peng
Chemical Communications, 2007 , # 9 p. 939 - 941
反应条件
1: With titanium tetrachloride in dichloromethane T=-60 - -20°C; 2: With toluene-4-sulfonic acid in dichloromethane T=20°C;
参考文献
Maslak, Veselin; Matovic, Radomir; Saicic, Radomir N.
Tetrahedron, 2004 , vol. 60, # 40 p. 8957 - 8966
反应条件
titanium tetrachloride in dichloromethane T=20°C; 4 h; Inert atmosphere;
参考文献
Zikou, Lamprini C.; Igglessi-Markopoulou, Olga
Synthesis, 2008 , # 12 art. no. T17907SS, p. 1861 - 1866
反应条件
titanium tetrachloride in dichloromethane T=25°C; 3 h;
参考文献
Zografos, Alexandros L.; Mitsos, Christos A.; Igglessi-Markopoulou, Olga
Organic Letters, 1999 , vol. 1, # 12 p. 1953 - 1955
反应条件
in dichloromethane; hexafluoroisopropyl alcohol T=20°C; 0.0833333 h; Inert atmosphere;
参考文献
Ratnikov, Maxim O.; Tumanov, Vasily V.; Smit, William A.
Angewandte Chemie - International Edition, 2008 , vol. 47, # 50 p. 9739 - 9742
反应条件
1.) CCl4, 3 h, 20 deg C; Yield given. Multistep reaction;
参考文献
Rousseau, Gerard; Blanco, Luis
Tetrahedron Letters, 1985 , vol. 26, # 35 p. 4191 - 4194
反应条件
ZnF2; tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium(0) in N,N-dimethyl-formamide T=80°C; 2 h;
参考文献
AMR Technology, Inc.
Patent: US2006/63808 A1, 2006 ;
Location in patent: Page/Page column 8; 10; 14 ;
反应条件
ZnF2; palladium(II) 2,4-pentanedionate; tri-tert-butyl phosphine in DMF (N,N-dimethyl-formamide) T=80°C; Product distribution / selectivity;
参考文献
AMR Technology, Inc.
Patent: US2006/63808 A1, 2006 ;
Location in patent: Page/Page column 9; 14 ;
反应条件
ZnF2; tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium(0) in N,N-dimethyl-formamide T=80°C;
参考文献
AMR Technology, Inc.
Patent: US2006/63808 A1, 2006 ;
Location in patent: Page/Page column 8; 10; 12; 14 ;
反应条件
iodosylbenzene Ambient temperature;
参考文献
Moriarty, Robert M.; Rani, Neena; Condeiu, Cristian; Duncan, Michael P.; Prakash, Om
Synthetic Communications, 1997 , vol. 27, # 18 p. 3273 - 3277