1-甲氧基-1-(三甲基甲硅氧基)-2-甲基-1-丙烯合成路线 (共 133 条)
反应条件
indium tribromide in dichloromethane
T=20°C; 2 h;
参考文献
Nishimoto, Yoshihiro; Yasuda, Makoto; Baba, Akio
Organic Letters, 2007 , vol. 9, # 24 p. 4931 - 4934
反应条件
1: With indium tribromide; trimethylsilyl bromide in dichloromethane
T=20°C; 2 h;
2: With water; sodium hydrogencarbonate
Saturated solution;
参考文献
Nishimoto, Yoshihiro; Saito, Takahiro; Yasuda, Makoto; Baba, Akio
Tetrahedron, 2009 , vol. 65, # 28 p. 5462 - 5471
反应条件
1: With indium tribromide; trimethylsilyl bromide in dichloromethane
T=20°C; 2 h;
2: With water; sodium hydrogencarbonate in dichloromethane
Saturated solution;
参考文献
Nishimoto, Yoshihiro; Saito, Takahiro; Yasuda, Makoto; Baba, Akio
Tetrahedron, 2009 , vol. 65, # 28 p. 5462 - 5471
反应条件
1: With indium tribromide; trimethylsilyl bromide in dichloromethane
T=20°C; 2 h;
2: With water; sodium hydrogencarbonate
Saturated solution;
参考文献
Nishimoto, Yoshihiro; Saito, Takahiro; Yasuda, Makoto; Baba, Akio
Tetrahedron, 2009 , vol. 65, # 28 p. 5462 - 5471
反应条件
1: With indium tribromide; trimethylsilyl bromide in dichloromethane
T=20°C; 2 h;
2: With water; sodium hydrogencarbonate
Saturated solution;
参考文献
Nishimoto, Yoshihiro; Saito, Takahiro; Yasuda, Makoto; Baba, Akio
Tetrahedron, 2009 , vol. 65, # 28 p. 5462 - 5471
反应条件
titanium tetrachloride in dichloromethane
T=20°C; Addition; Cyclization; 10 h;
参考文献
Allen, Martin P.; Blake, James F.; Bryce, Dianne K.; Haggan, Mary E.; Liras, Spiros; McLean, Stafford; Segelstein, Barb E.
Bioorganic and Medicinal Chemistry Letters, 2000 , vol. 10, # 6 p. 523 - 526
反应条件
triphenyl phosphite; [Ir(cod)2]SbF6 in 1,2-dichloro-ethane
T=20°C; Mannich reaction; 24 h; Inert atmosphere;
参考文献
Onodera, Gen; Toeda, Takayuki; Toda, Nou-No; Shibagishi, Daigo; Takeuchi, Ryo
Tetrahedron, 2010 , vol. 66, # 46 p. 9021 - 9031
反应条件
zinc dibromide in dichloromethane
Ambient temperature;
参考文献
Morrow, Gregory R.; Rae, Ian D.
Australian Journal of Chemistry, 1987 , vol. 40, # 8 p. 1477 - 1481
反应条件
P[2,4,6-(OMe)3C6H2]3 in N,N-dimethyl-formamide
T=20°C; 1 h;
参考文献
Matsukawa, Satoru; Obu, Kayoko
Chemistry Letters, 2004 , vol. 33, # 12 p. 1626 - 1627
反应条件
anhydrous lithium acetate in N,N-dimethyl-formamide
T=20°C; Mannich-type reaction; 6 h;
参考文献
Takahashi, Eiki; Fujisawa, Hidehiko; Yanai, Toshiharu; Mukaiyama, Teruaki
Chemistry Letters, 2005 , vol. 34, # 2 p. 216 - 217