1-乙氧基-2-甲基-1-(三甲基硅氧基)-1-丙烯合成路线 (共 24 条)
反应条件
[FeCp(CO)2Cl] in dichloromethane 48 h; Ambient temperature; Yield given;
参考文献
Colombo; Ulgheri; Prati
Tetrahedron Letters, 1989 , vol. 30, # 46 p. 6435 - 6436
反应条件
water; sodium amide 1.) 24 h, room t.; Yield given. Multistep reaction;
参考文献
Ali, Syed Masarrat; Tanimoto, Shigeo
Journal of the Chemical Society, Chemical Communications, 1988 , # 22 p. 1465 - 1466
反应条件
water; sodium amide 1.) 24 h, room t.; Yield given. Multistep reaction;
参考文献
Ali, Syed Masarrat; Tanimoto, Shigeo
Journal of the Chemical Society, Chemical Communications, 1988 , # 22 p. 1465 - 1466
反应条件
boron trifluoride diethyl etherate; diisobutylaluminium hydride 1) CH2Cl2/toluene, -78 deg C, 1 h, 2) CH2Cl2, -78 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Kiyooka, Syun-ichi; Shirouchi, Masashi
Journal of Organic Chemistry, 1992 , vol. 57, # 1 p. 1 - 2
反应条件
titanium tetrachloride in dichloromethane 2 h; Ambient temperature;
参考文献
Juaristi, Eusebio; Cruz-Sanchez, J. Samuel
Journal of Organic Chemistry, 1988 , vol. 53, # 14 p. 3334 - 3338
反应条件
trichlorophosphate 1.) CH2Cl2, 0-10 deg C, 30 min; 2.) room temp., 15 h; Yield given. Multistep reaction;
参考文献
Reddy, Chaganti P.; Tanimoto, Shigeo
Synthesis, 1987 , # 6 p. 575 - 577
反应条件
boron trifluoride diethyl etherate; diisobutylaluminium hydride 1) CH2Cl2/toluene, -78 deg C, 1 h, 2) CH2Cl2, -78 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Kiyooka, Syun-ichi; Shirouchi, Masashi
Journal of Organic Chemistry, 1992 , vol. 57, # 1 p. 1 - 2
反应条件
1: n-butyllithium / diethyl ether / -35 °C
2: triethylamine / methanol / 12 h / Heating
View Scheme
参考文献
Slougui, Nasser; Rousseau, Gerard; Conia, Jean-Marie
Synthesis, 1982 , # 1 p. 58 - 60
反应条件
boron trifluoride diethyl etherate; diisobutylaluminium hydride
1) CH2Cl2/toluene, -78 deg C, 1 h, 2) CH2Cl2, -78 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Kiyooka, Syun-ichi; Shirouchi, Masashi
Journal of Organic Chemistry, 1992 , vol. 57, # 1 p. 1 - 2
反应条件
boron trifluoride diethyl etherate; diisobutylaluminium hydride
1) CH2Cl2/toluene, -78 deg C, 1 h, 2) CH2Cl2, -78 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Kiyooka, Syun-ichi; Shirouchi, Masashi
Journal of Organic Chemistry, 1992 , vol. 57, # 1 p. 1 - 2