2,4,6-三羟基苯甲酸甲酯合成路线 (共 20 条)
反应条件
potassium carbonate in acetone T=20°C; 24 h;
参考文献
Journal of the American Chemical Society, , vol. 127, # 10 p. 3300 - 3309
反应条件
titanium(IV) isopropylate; titanium tetrachloride in dichloromethane 1.) -78 deg C, 5 h, 2.) RT, overnight;
参考文献
Journal of Organic Chemistry, , vol. 51, # 13 p. 2423 - 2428
参考文献
Monatshefte fuer Chemie, , vol. 23, p. 86
参考文献
Monatshefte fuer Chemie, , vol. 22, p. 219
参考文献
Monatshefte fuer Chemie, , vol. 22, p. 219
反应条件
1.1: DIPEA / CH2Cl2 / 4 h 1.2: 77 percent / NaH / dimethylformamide / 0.5 h 2.1: 96 percent / LiAlH4 / diethyl ether / 0 - 20 °C 3.1: 88 percent / tetrapropylammonium perruthenate; N-methylmorpholine-N-oxide / CH2Cl2 / 1 h View Scheme
参考文献
Henry, Kevin M.; Townsend, Craig A.
Journal of the American Chemical Society, 2005 , vol. 127, # 10 p. 3300 - 3309
反应条件
1: diethyl ether 2: diethyl ether 3: methanolic potash View Scheme
参考文献
Herzig; Wenzel; Toelk
Monatshefte fuer Chemie, 1902 , vol. 23, p. 86
反应条件
potassium carbonate; acetone
参考文献
Curd; Robertson
Journal of the Chemical Society, 1933 , p. 437,440
参考文献
Curd; Robertson
Journal of the Chemical Society, 1933 , p. 437,440
反应条件
potassium carbonate in acetone
T=15 - 20°C; 5 h;
参考文献
Schiemenz, Guenter Paulus; Behrens, Heinz; Ebert, Claus Peter; Maienschein, Konrad; Schroeder, Jens-Michael
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1985 , vol. 40, # 5 p. 681 - 692