4-羟基-2-甲基-6-苯甲基呋喃羧酸乙酯合成路线 （共 3 条）
反应条件
potassium carbonate in methanol; water T=20°C; 1 h;
参考文献
WO2004/46139 A1, ;
Page 26 ;
WO 2004/046139 A1
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; N-ethyl-N,N-diisopropylamine in N,N-dimethyl acetamide T=38°C; Sonogashira coupling; P=1277.21 Torr; 20 h; Inert atmosphereLarge scale reaction;
参考文献
Berliner, Martin A.; Cordi, Eric M.; Dunetz, Joshua R.; Price, Kristin E.
Organic Process Research and Development, 2010 , vol. 14, # 1 p. 180 - 187
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide T=24°C; P=1018.63 Torr; 25 h; Inert atmosphere;
参考文献
Organic Process Research and Development, , vol. 14, # 1 p. 180 - 187
