1: 92 percent / imidazole / dimethylformamide 2: 1) BuLi 3: Bu4NF / tetrahydrofuran / 2 h / 25 °C 4: 98 percent / NaH / dimethylformamide / 0.5 h / 50 °C View Scheme
参考文献
Ayrey, Peter M.; Bolton, Michael A.; Buss, Antony D.; Greeves, Nicholas; Levin, Daniel; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 24 p. 3407 - 3418
1: 1) BuLi 2: Bu4NF / tetrahydrofuran / 2 h / 25 °C 3: 98 percent / NaH / dimethylformamide / 0.5 h / 50 °C View Scheme
参考文献
Ayrey, Peter M.; Bolton, Michael A.; Buss, Antony D.; Greeves, Nicholas; Levin, Daniel; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 24 p. 3407 - 3418
1: 94 percent / LiBH4 / tetrahydrofuran 2: 92 percent / imidazole / dimethylformamide 3: 1) BuLi 4: Bu4NF / tetrahydrofuran / 2 h / 25 °C 5: 98 percent / NaH / dimethylformamide / 0.5 h / 50 °C View Scheme
参考文献
Ayrey, Peter M.; Bolton, Michael A.; Buss, Antony D.; Greeves, Nicholas; Levin, Daniel; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 24 p. 3407 - 3418