Alpha-甲基苯乙酸甲酯合成路线 (共 146 条)
反应条件
1-methoxy-2-phenylprop-1-enolate in tetrahydrofuran T=-78°C; 1 h; other reagent; Product distribution;
参考文献
Differding, Edmond; Lang, Robert W.
Helvetica Chimica Acta, 1989 , vol. 72, p. 1248 - 1252
反应条件
hydrogen; (p-toluenesulfonate)2palladium*1,3-bis(diphenylphosphino)propane T=100°C; P=30002.4 Torr; 4 h; var. of catalyst, its conc., solvent, partial pressure, temp., time, further with var. amounts of p-TsOH*H2O or H2O; Product distributionMechanism;
参考文献
Pisano, Carmelina; Consiglio, Giambattista
Gazzetta Chimica Italiana, 1994 , vol. 124, # 10 p. 393 - 402
反应条件
[Ni(1,2-bis(di-isopropylphosphino)ethane)(μ-H)]2 in tetrahydrofuran T=120°C; 36 h; Schlenk techniqueInert atmosphere; Catalytic behavior; Reagent/catalyst;
参考文献
Gonzalez-Sebastian, Lucero; Flores-Alamo, Marcos; Garcia, Juventino J.
Organometallics, 2012 , vol. 31, # 23 p. 8200 - 8207
反应条件
[Ni(1,2-bis(di-isopropylphosphino)ethane)(μ-H)]2 in tetrahydrofuran T=120°C; 36 h; Schlenk techniqueInert atmosphere; Catalytic behavior; Concentration;
参考文献
Gonzalez-Sebastian, Lucero; Flores-Alamo, Marcos; Garcia, Juventino J.
Organometallics, 2012 , vol. 31, # 23 p. 8200 - 8207
反应条件
t-BuOK in tert-butyl alcohol T=185°C; Product distribution;
参考文献
Dyllick-Brenzinger, Rainer A.; Patel, Vijay; Rampersad, Mollin B.; Stothers, J. B.; Thomas, Shirley E.
Canadian Journal of Chemistry, 1990 , vol. 68, # 7 p. 1106 - 1115
反应条件
1: (i) NaH, DMF, (ii) /BRN= 969135/, (iii) KOH, EtOH 2: (i) KOH, EtOH, (ii) /BRN= 1098229/ View Scheme
参考文献
des Albayes,H.
Bulletin de la Societe Chimique de France, 1970 , p. 3671 - 3678
反应条件
(i) KOH, EtOH, (ii) /BRN= 1098229/; Multistep reaction;
参考文献
des Albayes,H.
Bulletin de la Societe Chimique de France, 1970 , p. 3671 - 3678
反应条件
[Ni(1,2-bis(di-isopropylphosphino)ethane)(μ-H)]2 in tetrahydrofuran T=120°C; 36 h; Schlenk techniqueInert atmosphere; Catalytic behavior;
参考文献
Gonzalez-Sebastian, Lucero; Flores-Alamo, Marcos; Garcia, Juventino J.
Organometallics, 2012 , vol. 31, # 23 p. 8200 - 8207
反应条件
N(Et)4ClO4 in N,N-dimethyl-formamide 20 h; electrolysis, -2.0 V;
参考文献
Luca, Carlo de; Inesi, Achille; Rampazzo, Liliana
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1982 , p. 1403 - 1408
反应条件
potassium carbonate T=195°C; 6.4 h; other ketones, other dialkyl carbonate; other temperature and time; Product distributionMechanism;
参考文献
Selva, Maurizio; Marques, Carlos Alberto; Tundo, Pietro
Gazzetta Chimica Italiana, 1993 , vol. 123, # 9 p. 515 - 518