Alpha-甲基苯乙酸甲酯合成路线 (共 146 条)
反应条件
p-Ts; triphenylphosphine; copper dichloride; palladium dichloride in 1,4-dioxane T=100°C; P=45003.6 Torr; 24 h; effect of the amount of p-Ts on carbonylation reaction; also further substrate investigated; Product distribution;
参考文献
Zhou, Hongying; Cheng, Jing; Lu, Shijie; Fu, Hongxiang; Wang, Hanqing
Journal of Organometallic Chemistry, 1998 , vol. 556, # 1-2 p. 239 - 242
反应条件
hydrogen; [rhodium(I)(carbonyl)2(acetylacetonate)]; (Me)CgPPh in toluene T=100°C; P=3750.3 Torr; 70 h;
参考文献
Clarke, Matthew L.; Roff, Geoffrey J.
Chemistry - A European Journal, 2006 , vol. 12, # 31 p. 7979 - 7986
反应条件
hydrogen; [rhodium(I)(carbonyl)2(acetylacetonate)]; (Me)CgPPh in toluene T=30°C; P=37503 Torr; 90 h;
参考文献
Clarke, Matthew L.; Roff, Geoffrey J.
Chemistry - A European Journal, 2006 , vol. 12, # 31 p. 7979 - 7986
反应条件
1) EGB.2 T=-78°C; other methyl arylacetates, other halogenides;
参考文献
Shono, Tatsuya; Kashimura, Shigenori; Nogusa, Hideo
Journal of Organic Chemistry, 1984 , vol. 49, # 11 p. 2043 - 2045
反应条件
lead(IV) acetate; perchloric acid in various solvent(s) T=25°C; 30 h;
参考文献
Yamauchi, Takayoshi; Nakao, Kenji; Fujii, Kyoichi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1433 - 1436
反应条件
toluene-4-sulfonic acid; [PdCl(Ph2PNHpy-κ2P,N)(PPh3)]Cl in toluene T=80°C; P=37503.8 Torr;
参考文献
Aguirre, Pedro A.; Lagos, Carolina A.; Moya, Sergio A.; Zuniga, Cesar; Vera-Oyarce, Cristian; Sola, Eduardo; Peris, Gabriel; Bayon, J. Carles
Dalton Transactions, 2007 , # 46 p. 5419 - 5426
反应条件
1: (+/-)-2-Phenylpropionic acid With 1,8-diazabicyclo[5.4.0]undec-7-ene in toluene T=20°C; 1 h; 2: methyl iodide in toluene T=20°C;
参考文献
Kulig; Ignasik; Malawska
Polish Journal of Chemistry, 2009 , vol. 83, # 9 p. 1629 - 1636
反应条件
hydrogen; Co catalyst
参考文献
Marsh, Barrie J.; Carbery, David R.
Journal of Organic Chemistry, 2009 , vol. 74, # 8 p. 3186 - 3188
反应条件
manganese; NiBr2bipy; trifluoroacetic acid in N,N-dimethyl-formamide T=20°C; 1 h;
参考文献
Durandetti, Muriel; Gosmini, Corinne; Perichon, Jacques
Tetrahedron, 2007 , vol. 63, # 5 p. 1146 - 1153
反应条件
mercury dichloride; mercury(II) oxide in methanol; water 5 h; Heating;
参考文献
Halfpenny, Paul R.; Horwell, David C.; Rees, David C.
Synthesis, 1990 , # 6 p. 517 - 519