Alpha-甲基苯乙酸甲酯合成路线 (共 146 条)
反应条件
perchloric acid; thallium(III) nitrate T=50°C; 10 h; various time and temp.; Product distribution;
参考文献
Yamauchi, Takayoshi; Nakao, Kenji; Fujii, Kyoichi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1255 - 1258
反应条件
RhH2(O2COH)(P(i-Pr)3)2 in tetrahydrofuran T=120°C; 20 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Okano, Tamon; Kobayashi, Teruyuki; Konishi, Hisatoshi; Kiji, Jitsuo
Tetrahedron Letters, 1982 , vol. 23, # 47 p. 4967 - 4968
反应条件
iodine; silver nitrate 5 h; Heating;
参考文献
Higgins, Stanley D.; Thomas, Barry C.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 235 - 242
反应条件
1: Jones reagent 2: SOCl2 View Scheme
参考文献
Sugai, Saburo; Kodama, Takashi; Akaboshi, Sanya; Ikegami, Shiro
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 1 p. 99 - 105
反应条件
potassium acetate in water; N,N-dimethyl-formamide 14 h; HeatingVar.: solv., base, temp. and time;
参考文献
Tsuchihashi, Gen-ichi; Kitajima, Koji; Mitamura, Shuichi
Tetrahedron Letters, 1981 , vol. 22, # 43 p. 4305 - 4308
反应条件
boron trifluoride; silver carbonate T=15°C; 20 h;
参考文献
Giordano, Claudio; Castaldi, Graziano; Uggeri, Fulvio; Gurzoni, Francesco
Synthesis, 1985 , # 4 p. 436 - 437
反应条件
bis-triphenylphosphine-palladium(II) chloride T=110°C; P=15001.2 Torr; 4 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kron; Terekhova; Noskov; Petrov
Russian Journal of General Chemistry, 1997 , vol. 67, # 1 p. 102 - 105
反应条件
1: 75 percent / BuLi / tetrahydrofuran / 1) -78 deg C, 2h, 2) room temperature 2: 75 percent / HgO/HgCl2 / methanol; H2O / 5 h / Heating View Scheme
参考文献
Halfpenny, Paul R.; Horwell, David C.; Rees, David C.
Synthesis, 1990 , # 6 p. 517 - 519
反应条件
1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h 2: tetrahydrofuran / 1 h 3: UV-irradiation View Scheme
参考文献
Shiraki, Saori; Natarajan, Arunkumar; Garcia-Garibay, Miguel A.
Photochemical and Photobiological Sciences, 2011 , vol. 10, # 9 p. 1480 - 1487
反应条件
3-chloro-benzenecarboperoxoic acid T=25°C; 24 h;
参考文献
Uemura, Sakae; Ohe, Kouichi; Yamauchi, Takayoshi; Mizutaki, Shoichi; Tamaki, Kentaro
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 4 p. 907 - 910