in tetrahydrofuran a soln. of PhCH2MgCl was treated with soln. of (PhCH2)3SnCl, a mixture was stirred and refluxed for 18 h; hydrolysis with cold water, evapn. in vac., crystn. (pertoleum ether); elem. anal.;
参考文献
Legzdins, Peter; Martin, David T.
Organometallics, 1983 , vol. 2, p. 1785 - 1791
Bhattacharya, S. N.; Prem Raj,; Saxena, A. K.
Indian J. Chem. A, 1978 , vol. 16, p. 1071 - 1074
Full Text Show Details
Gmelin Handbook: S: SVol.4a/b, 1.3.12, page 303 - 305
in tetrahydrofuran byproducts: NaCl; addn. of tribenzyltin chloride to cerate soln. with stirring (Ar); react., 12h; filtration; evapn.; dissoln. of residue with addn. of activated carbon and Al2O3 (pentane); hot filtration; evapn.; crystn.; filtration; drying (vac.); elem. anal.;
参考文献
Jacob, K.; Glanz, M.; Holecek, J.; Lycka, A.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1990 , vol. 581, p. 33 - 40
