5,6-二氢-4H-吡喃-2-甲腈合成路线 (共 8 条)
参考文献
Clive, Derrick L. J.; Minaruzzaman; Yang, Haikang
Organic Letters, 2005 , vol. 7, # 25 p. 5581 - 5583
反应条件
piperidine in tetrachloromethane 60 h; Ambient temperature; Yield given;
参考文献
Synthesis, , # 7 p. 548 - 551
反应条件
1: Br2 / CCl4 / 1.) -6 to -12 deg C, 2.) room temp., 1.5 h 2: CCl4 / 16 h / Heating 3: piperidine / CCl4 / 60 h / Ambient temperature View Scheme
参考文献
Synthesis, , # 7 p. 548 - 551
反应条件
1: CCl4 / 16 h / Heating 2: piperidine / CCl4 / 60 h / Ambient temperature View Scheme
参考文献
Synthesis, , # 7 p. 548 - 551
反应条件
1: potassium hydroxide / water / 12 h 2: caesium carbonate; hydrogen; C63H78IrNOP(2+)*C32H12BF24(1-) / methanol / 12 h / 60 °C / 4560.31 Torr / |Autoclave View Scheme
参考文献
Song, Song; Zhu, Shou-Fei; Pu, Liu-Yang; Zhou, Qi-Lin
Angewandte Chemie - International Edition, 2013 , vol. 52, # 23 p. 6072 - 6075
Angew. Chem., 2013 , vol. 125, # 23 p. 6188 - 6191
反应条件
potassium hydroxide in water
参考文献
Clive, Derrick L. J.; Minaruzzaman; Yang, Haikang
Organic Letters, 2005 , vol. 7, # 25 p. 5581 - 5583
反应条件
1: 97 percent / KOH / H2O 2: 81 percent / NaHCO3 / methanol View Scheme
参考文献
Organic Letters, , vol. 7, # 25 p. 5581 - 5583
反应条件
diisobutylaluminium hydride in toluene
参考文献
BASF Aktiengesellschaft
Patent: US5536734 A1, 1996 ;