5,6-二氢-4H-吡喃-2-甲酸合成路线 （共 16 条）
反应条件
C63H78IrNOP(2+)*C32H12BF24(1-); hydrogen; caesium carbonate in methanol T=60°C; P=4560.31 Torr; 12 h; Autoclave; enantioselective reaction;
参考文献
Song, Song; Zhu, Shou-Fei; Pu, Liu-Yang; Zhou, Qi-Lin
Angewandte Chemie - International Edition, 2013 , vol. 52, # 23 p. 6072 - 6075
Angew. Chem., 2013 , vol. 125, # 23 p. 6188 - 6191
反应条件
ethyl acetate; platinum Hydrogenation;
参考文献
Paul; Tchelitcheff
Bulletin de la Societe Chimique de France, 1952 , p. 808,812
反应条件
sodium hydrogencarbonate in methanol
参考文献
Organic Letters, , vol. 7, # 25 p. 5581 - 5583
反应条件
1: potassium hydroxide / benzene / 12 h / Heating
2: 74 percent / lithium aluminum hydride / diethyl ether / 1 h
View Scheme
参考文献
Bouchu, D.; Dreux, J.
Phosphorus and Sulfur and the Related Elements, 1982 , vol. 13, p. 25 - 34
反应条件
sulfuric acid
2 h; Reflux;
参考文献
Murugan, Kaliyappan; Srimurugan, Sankareswaran; Chen, Chinpiao
Chemical Communications, 2010 , vol. 46, # 7 p. 1127 - 1129
反应条件
potassium hydroxide in benzene
12 h; Heating; Yield given;
参考文献
Bouchu, D.; Dreux, J.
Phosphorus and Sulfur and the Related Elements, 1982 , vol. 13, p. 25 - 34
