2-甲氧基[2-乙氧基(2-乙氧基)]-1-乙硫醇合成路线 （共 10 条）
反应条件
hydrogenchloride in methanol; water T=100°C; 2.5 h;
参考文献
Keddie, Daniel J.; Grande, John B.; Gonzaga, Ferdinand; Brook, Michael A.; Dargaville, Tim R.
Organic Letters, 2011 , vol. 13, # 22 p. 6006 - 6009
反应条件
1: With thiourea in ethanol; water 3 h; RefluxInert atmosphere; 2: With sodium hydroxide in ethanol; water 2 h; RefluxInert atmosphere;
参考文献
Ruizendaal, Loes; Pujari, Sidharam P.; Gevaerts, Veronique; Paulusse, Jos M. J.; Zuilhof, Han
Chemistry - An Asian Journal, 2011 , vol. 6, # 10 p. 2776 - 2786
反应条件
1.1: 42 percent / phosphorus tribromide / 24 h / 20 °C 2.1: ethanol / 8 h / Heating 2.2: 67 percent / aq.NaOH / 1 h / Heating View Scheme
参考文献
Keddie, Daniel J.; Grande, John B.; Gonzaga, Ferdinand; Brook, Michael A.; Dargaville, Tim R.
Organic Letters, 2011 , vol. 13, # 22 p. 6006 - 6009
反应条件
1: in ethanol 8 h; Heating; 2: With sodium hydroxide 1 h; Heating; Further stages.;
参考文献
Dabak, Salih; Ahsen, Vefa; Heinemann, Frauke; Zugenmaier, Peter
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 2000 , vol. 348, p. 111 - 127
反应条件
1: acetone / 50 °C 2: sodium hydroxide; hydrogenchloride / methanol; ethanol; water / 0.92 h / |Inert atmosphere 3: acetone / |Reflux 4: sodium hydroxide; hydrogenchloride / methanol; ethanol; water / 0.92 h / |Inert atmosphere View Scheme
参考文献
Gobbo, Pierangelo; Novoa, Samantha; Biesinger, Mark C.; Workentin, Mark S.
Chemical Communications, 2013 , vol. 49, # 38 p. 3982 - 3984
反应条件
1: sodium azide / acetonitrile / |Reflux 2: acetone / 50 °C 3: sodium hydroxide; hydrogenchloride / methanol; ethanol; water / 0.92 h / |Inert atmosphere 4: acetone / |Reflux 5: sodium hydroxide; hydrogenchloride / methanol; ethanol; water / 0.92 h / |Inert atmosphere View Scheme
参考文献
Gobbo, Pierangelo; Novoa, Samantha; Biesinger, Mark C.; Workentin, Mark S.
Chemical Communications, 2013 , vol. 49, # 38 p. 3982 - 3984
反应条件
1: sodium hydroxide; hydrogenchloride / methanol; ethanol; water / 0.92 h / |Inert atmosphere 2: acetone / |Reflux 3: sodium hydroxide; hydrogenchloride / methanol; ethanol; water / 0.92 h / |Inert atmosphere View Scheme
参考文献
Gobbo, Pierangelo; Novoa, Samantha; Biesinger, Mark C.; Workentin, Mark S.
Chemical Communications, 2013 , vol. 49, # 38 p. 3982 - 3984
反应条件
1: acetone / |Reflux 2: sodium hydroxide; hydrogenchloride / methanol; ethanol; water / 0.92 h / |Inert atmosphere View Scheme
参考文献
Gobbo, Pierangelo; Novoa, Samantha; Biesinger, Mark C.; Workentin, Mark S.
Chemical Communications, 2013 , vol. 49, # 38 p. 3982 - 3984
反应条件
1: triethylamine; 4-(N,N-dimethlyamino)pyridine / dichloromethane / 4 h / 0 - 20 °C 2: sodium azide / acetonitrile / |Reflux 3: acetone / 50 °C 4: sodium hydroxide; hydrogenchloride / methanol; ethanol; water / 0.92 h / |Inert atmosphere 5: acetone / |Reflux 6: sodium hydroxide; hydrogenchloride / methanol; ethanol; water / 0.92 h / |Inert atmosphere View Scheme
参考文献
Gobbo, Pierangelo; Novoa, Samantha; Biesinger, Mark C.; Workentin, Mark S.
Chemical Communications, 2013 , vol. 49, # 38 p. 3982 - 3984
反应条件
sodium t-butanolate in methanol T=20°C; 0.5 h; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 64, # 9 p. 3106 - 3112
