2-甲氧基-4-硝基苯硫酚合成路线 (共 3 条)
反应条件
1: With trifluoromethylsulfonic anhydride; triethylamine in dichloromethane T=0 - 20°C; 1 h; 2: With sulfur; sodium sulfate in ethanol; water 0.333333 h; 3: With hydrogenchloride; sodium hydroxide more than 3 stages;
参考文献
Takeda Chemical Industries, Ltd.
Patent: EP1422228 A1, 2004 ;
Location in patent: Page 204 ;
EP 1422228 A1
参考文献
Amgen Inc.
Patent: US2005/250820 A1, 2005 ;
Location in patent: Page/Page column 71 ;
US 20050250820 A1
反应条件
iron; acetic acid
T=20°C; 6 h;
参考文献
Takeda Chemical Industries, Ltd.
Patent: EP1422228 A1, 2004 ;
Location in patent: Page 204 ;
EP 1422228 A1