1-(3-乙氧基-4-甲氧基苯基)乙酮合成路线 (共 11 条)
反应条件
potassium carbonate in N,N-dimethyl-formamide T=100°C; 6 h;
参考文献
Rosiak, Anna; Frey, Wolfgang; Christoffers, Jens
European Journal of Organic Chemistry, 2006 , # 17 p. 4044 - 4054
反应条件
Dess-Martin periodane in dichloromethane T=20°C; 4 h;
参考文献
NOVARTIS AG; NOVARTIS PHARMA GMBH
Patent: WO2007/20046 A1, 2007 ;
Location in patent: Page/Page column 44 ;
WO 2007/020046 A1
参考文献
Kobayashi, Shigeru; Okimoto, Kazuto; Imakura, Yasuhiro
Chemical & Pharmaceutical Bulletin, 1982 , vol. 30, # 5 p. 1567 - 1573
反应条件
Hβ zeolite (Si:Al 12.5) T=120°C; 3 h; Title compound not separated from byproducts.;
参考文献
Smith, Keith; El-Hiti, Gamal A.; Jayne, Anthony J.; Butters, Michael
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 9 p. 1560 - 1564
反应条件
1: SOCl2 / 0.5 h / Heating 2: Na-ethoxide / ethanol 3: H2SO4 / 8 h / Heating View Scheme
参考文献
Ahluwalia, V. K.; Kapur, Kanchan; Manchanda, Saroj
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 3 p. 186 - 188
参考文献
Reichstein
Helvetica Chimica Acta, 1927 , vol. 10, p. 389
反应条件
1: 0.2 g / hydrobromic acid / 3 h / Heating 2: K2CO3 View Scheme
参考文献
Ahluwalia, V. K.; Kapur, Kanchan; Manchanda, Saroj
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 3 p. 186 - 188
参考文献
Ahluwalia, V. K.; Kapur, Kanchan; Manchanda, Saroj
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 3 p. 186 - 188
参考文献
Kondo; Tanaka
Yakugaku Zasshi, 1929 , vol. 49, p. 49
Chem. Zentralbl., 1929 , vol. 100, # I p. 2978
Full Text Show Details
Kondo; Tanaka; Noto
Yakugaku Zasshi, 1928 , vol. 48, p. 168
Yakugaku Zasshi, 1929 , vol. 49, p. 49
Chem. Zentralbl., 1929 , vol. 100, # I p. 1112,2978
反应条件
1: permanganate; alkali 2: Cr2O3-H2SO4 View Scheme
参考文献
Reichstein
Helvetica Chimica Acta, 1927 , vol. 10, p. 389