3-(溴甲基)-2,5-二氢噻吩 1,1-二氧化物合成路线 （共 5 条）
参考文献
Chae, Woo-Ki; Baughman, Sharon A.; Engel, Paul S.; Bruch, Manfred; Oezmeral, Cenan; et al.
Journal of the American Chemical Society, 1981 , vol. 103, # 16 p. 4824 - 4833
反应条件
1: 160 - 165 °C / 10 Torr
2: ethanol
3: LiAlH4 / diethyl ether
View Scheme
参考文献
Thomas,A.F.
Journal of the American Chemical Society, 1969 , vol. 91, p. 3281 - 3289
反应条件
1: 94 percent / aq. KOH / dioxane / Ambient temperature
2: 82 percent / H2O2 / acetone
View Scheme
参考文献
Tolstikov, G. A.; Novitskaya, N. N.; Shul'ts, E. E.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 1447 - 1452
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 8 p. 1636 - 1641
反应条件
potassium hydroxide in 1,4-dioxane
Ambient temperature;
参考文献
Tolstikov, G. A.; Novitskaya, N. N.; Shul'ts, E. E.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 1447 - 1452
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 8 p. 1636 - 1641
反应条件
1: 94 percent / aq. KOH / dioxane / Ambient temperature
2: 82 percent / H2O2 / acetone
3: 90 percent / SOCl2 / CCl4 / 0.5 h / Ambient temperature
View Scheme
参考文献
Tolstikov, G. A.; Novitskaya, N. N.; Shul'ts, E. E.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 1447 - 1452
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 8 p. 1636 - 1641
