(S)-(-)-叔丁烷硫代亚磺酸叔丁酯合成路线 (共 34 条)
反应条件
dihydrogen peroxide in acetic acid T=25 - 37°C; 3 - 8.15 h;
参考文献
EP1484301 A1, ;
Page 16; 19 ;
反应条件
bis(2-pyridinyl)sulfoxide in tetrahydrofuran T=-95°C;
参考文献
Journal of Organic Chemistry, , vol. 56, # 22 p. 6341 - 6348
反应条件
T=340°C; flash vacuum pyrolysis;
参考文献
Journal of Organic Chemistry, , vol. 46, # 17 p. 3467 - 3474
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane 1.) 22 - 24 deg C, 30 min, 2.) reflux, 1 h; Further byproducts given;
参考文献
Journal of Organic Chemistry, , vol. 53, # 6 p. 1263 - 1266
反应条件
phenyl-magnesium bromide in tetrahydrofuran 0.25 h; Ambient temperature;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 27, p. 13 - 30
参考文献
Journal of the American Chemical Society, , vol. 103, # 23 p. 7016 - 7018
反应条件
1H-imidazole; manganese(II) tetraphenylporphyrinate; tetra-n-butylammonium monopersulfate in dichloromethane T=20°C; 0.0166667 h;
参考文献
Tetrahedron Letters, , vol. 45, # 19 p. 3811 - 3815
反应条件
in toluene T=340°C; flash vacuum pyrolysis;
参考文献
Journal of Organic Chemistry, , vol. 46, # 17 p. 3467 - 3474
反应条件
in tetrahydrofuran 0.25 h; Ambient temperature;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 34, p. 123 - 132
Phosphorus and Sulfur and the Related Elements, , vol. 27, p. 13 - 30
反应条件
pyridine in diethyl ether
参考文献
Journal of the Chemical Society, , p. 5339 - 5344