三(2,4-二叔丁基苯基)亚磷酸酯合成路线 （共 7 条）
反应条件
N,N-dimethyl-n-dodecylamine; phosphorus trichoride T=90 - 200°C; P=37.5038 - 750.075 Torr; Inert atmosphere; Product distribution / selectivity;
参考文献
WO2011/14527 A2, ;
Page/Page column 36; 37 ;
反应条件
in chlorobenzene T=29.9°C; Rate constantMechanism;
参考文献
Koenig, T.; Habicher, W. D.; Schwetlick, K.
Journal fuer Praktische Chemie (Leipzig), 1989 , vol. 331, # 6 p. 913 - 922
反应条件
triethanolamine in toluene
参考文献
Kuraray Co., Ltd.
Patent: US6331650 B1, 2001 ;
反应条件
in 2-methoxy-ethanol all manipulations under N2 atm.; soln. of PdCl2 and ligand refluxed for 2 h; filtered, EtOH added, concd. in vac.;
参考文献
Bedford, Robin B.; Betham, Michael; Coles, Simon J.; Horton, Peter N.; Lopez-Saez, Maria-Jose
Polyhedron, 2006 , vol. 25, # 4 p. 1003 - 1010
反应条件
in dichloromethane all manipulations under N2 atm.; soln. of P and Pd compds. stirred for 1.5 h at room temp.; MeOH added, concd. in vac.;
参考文献
Bedford, Robin B.; Betham, Michael; Coles, Simon J.; Horton, Peter N.; Lopez-Saez, Maria-Jose
Polyhedron, 2006 , vol. 25, # 4 p. 1003 - 1010
反应条件
iodine in tetrahydrofuran; water
T=20°C; 1 h;
参考文献
Sano, Takahiro; Senzaki, Hirohiko; Sugaya, Toru; Kasai, Masaji
Organic Process Research and Development, 2000 , vol. 4, # 5 p. 349 - 352
反应条件
in chlorobenzene
T=29.9°C; Rate constantMechanism;
参考文献
Koenig, T.; Habicher, W. D.; Schwetlick, K.
Journal fuer Praktische Chemie (Leipzig), 1989 , vol. 331, # 6 p. 913 - 922
