2-(2-甲氧基乙氧基)乙胺合成路线 （共 10 条）
反应条件
hydrogen; palladium on activated charcoal in methanol P=5250.4 Torr; 4 h;
参考文献
Seguer, J.; Selve, C.; Allouch, M.; Infante, M. R.
Journal of the American Oil Chemists' Society, 1996 , vol. 73, # 1 p. 79 - 86
反应条件
1: With sodium azide in N,N-dimethyl-formamide T=67°C; 10 h; Inert atmosphere; 2: With triphenylphosphine in diethyl ether T=0 - 20°C; 2.5 h;
参考文献
Clerc, Jerome; Schellenberg, Barbara; Groll, Michael; Bachmann, Andre S.; Huber, Robert; Dudler, Robert; Kaiser, Markus
European Journal of Organic Chemistry, 2010 , # 21 p. 3991 - 4003
反应条件
NH2NH2•xH2O in ethanol T=76°C; Gabriel's dephthaloylation; 3 h;
参考文献
Harjani, Jitendra R.; Liang, Chen; Jessop, Philip G.
Journal of Organic Chemistry, 2011 , vol. 76, # 6 p. 1683 - 1691
反应条件
ammonia in methanol T=120 - 130°C; 4 h; Sealed tube;
参考文献
US2010/298351 A1, ;
Page/Page column 35 ;
US 20100298351 A1
反应条件
1: 84 percent / pyridine / 12 h / 0 °C 2: 80 percent / NaN3 / dimethylformamide / 65 °C 3: LiAlH4 / diethyl ether / 6 h / Heating View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 13, # 7 p. 1381 - 1384
反应条件
trifluoroacetic acid in dichloromethane 0.5 h;
参考文献
US2004/87601 A1, ;
Page 29 ;
US 20040087601 A1
反应条件
1: sodium azide, NaI / dimethylformamide / 18 h / 60 °C 2: 1.) Ph3P, 2.) H2O / 1.) THF, RT, 10 h, 2.) THF, RT, 24 h View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 38, # 7 p. 1067 - 1083
反应条件
(i) phthalimide <K salt>, (ii) N2H4*H2O; Multistep reaction;
参考文献
Chemische Berichte, , vol. 112, p. 1392 - 1399
反应条件
hydrazine hydrate in ethanol 3 h; Reflux;
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 5 p. 1152 - 1155
反应条件
pyridine
65 h; Heating;
参考文献
Wiest, Olaf; Harrison, Christopher B.; Saettel, Nicolas J.; Cibulka, Radek; Sax, Mirjam; Koenig, Burkhard
Journal of Organic Chemistry, 2004 , vol. 69, # 24 p. 8183 - 8185
