10,11-二氢二苯并[b,f][1,4]噁杂-11-酮合成路线 (共 34 条)
反应条件
T=215°C; bzw. 250grad;
参考文献
Journal of the American Chemical Society, , vol. 56, p. 117,118
反应条件
sodium hydroxide in N,N-dimethyl-formamide 5 h; Heating;
参考文献
Journal of Medicinal Chemistry, , vol. 49, # 15 p. 4512 - 4516
反应条件
1: Et3N / tetrahydrofuran / 0 - 20 °C 2: NaOH / dimethylformamide / 5 h / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 49, # 15 p. 4512 - 4516
反应条件
1: thionyl chloride / 2 h / Heating 2: Et3N / tetrahydrofuran / 0 - 20 °C 3: NaOH / dimethylformamide / 5 h / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 49, # 15 p. 4512 - 4516
反应条件
1: (i-Pr)2NEt / tetrahydrofuran / 48 h / 25 °C 2: KOMe / various solvent(s) / 275 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 35, # 10 p. 1887 - 1897
反应条件
1: (i-Pr)2NEt / tetrahydrofuran / 48 h / 25 °C 2: KOMe / various solvent(s) / 275 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 35, # 10 p. 1887 - 1897
反应条件
1: platinum / Hydrogenation 2: 215 °C / bzw. 250grad View Scheme
参考文献
Journal of the American Chemical Society, , vol. 56, p. 117,118
反应条件
1: sodium dichromate; sulfuric acid 2: platinum / Hydrogenation 3: 215 °C / bzw. 250grad View Scheme
参考文献
Journal of the American Chemical Society, , vol. 56, p. 117,118
反应条件
1: 170 °C / weiteres Erhitzen auf 190-200grad 2: sodium dichromate; sulfuric acid 3: platinum / Hydrogenation 4: 215 °C / bzw. 250grad View Scheme
参考文献
Journal of the American Chemical Society, , vol. 56, p. 117,118
反应条件
phosphorus pentachloride in diethyl ether Ambient temperature;
参考文献
Indian Journal of Chemistry, , vol. 12, p. 247 - 251