2-氯二苯并[b,f][1,4]氧氮杂卓-11(10H)-酮合成路线 (共 3 条)
反应条件
4-(N,N-dimethlyamino)pyridine; sodium carbonate; bis(dibenzylideneacetone)-palladium(0); di-(1-adamantyl)-n-butylphosphine in toluene T=80°C; Inert atmosphereSealed chamber;
参考文献
Hermange, Philippe; Lindhardt, Anders T.; Taaning, Rolf H.; Bjerglund, Klaus; Lupp, Daniel; Skrydstrup, Troels
Journal of the American Chemical Society, 2011 , vol. 133, # 15 p. 6061 - 6071
反应条件
hydrogenchloride 16 h; Heating;
参考文献
Helvetica Chimica Acta, , vol. 50, p. 245 - 254
反应条件
1: POCl3, PhNMe2 / 5 h / Heating 2: xylene / 5 h / Heating View Scheme
参考文献
Schmutz,J. et al.
Helvetica Chimica Acta, 1967 , vol. 50, p. 245 - 254