二苯并[b,f][1,4]硫氮杂卓-11-[10H]酮合成路线 （共 38 条）
参考文献
Polivka; Holubek; Svatek; et al.
Collection of Czechoslovak Chemical Communications, 1983 , vol. 48, # 5 p. 1465 - 1476
反应条件
AlCl3, aluminium chloride in 1,2-dichloro-benzene T=100 - 150°C; 4 h;
参考文献
ELI LILLY AND COMPANY
Patent: WO2005/26177 A1, 2005 ;
Location in patent: Page/Page column 75 ;
WO 2005/026177 A1
反应条件
polyphosphoric acid Heating;
参考文献
Mahale, Ganesh D.; Kolekar, Yogesh M.; Kumar, Ashok; Singh, Dharmendra; Kodam, Kisan M.; Waghmode, Suresh B.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2011 , vol. 50, # 9 p. 1196 - 1201
反应条件
acetic acid in anhydrous xylene; water
反应条件
acetic acid T=135°C;
参考文献
Panda, Niranjan; Jena, Ashis Kumar; Mohapatra, Sasmita
Applied Catalysis A: General, 2012 , vol. 433-434, p. 258 - 264
反应条件
potassium hydroxide; copper in water
反应条件
copper(II) ferrite; potassium tert-butylate in N,N-dimethyl-formamide 24 h; RefluxInert atmosphere;
参考文献
Panda, Niranjan; Jena, Ashis Kumar; Mohapatra, Sasmita
Applied Catalysis A: General, 2012 , vol. 433-434, p. 258 - 264
反应条件
trifluoroacetic anhydride in N,N-dimethyl-formamide 1.) reflux, 1 h, 2.) RT, overnight;
参考文献
Kuti, M.; Rabai, J.; Kapovits, I.
Phosphorus, Sulfur and Silicon and the Related Elements, 1993 , vol. 85, # 1-4 p. 119 - 128
反应条件
1: methanol. sodium methylate 2: ethyl acetate; Raney nickel / Hydrogenation 3: 220 °C View Scheme
参考文献
Helvetica Chimica Acta, , vol. 42, p. 1265,1269,1272
反应条件
in tert-butyl alcohol 2 h; Irradiation;
参考文献
Kamigata, Nobumasa; Hashimoto, Satoshi; Fujie, Shin-ichi; Kobayashi, Michio
Journal of the Chemical Society, Chemical Communications, 1983 , # 13 p. 765 - 766
