(E)-4-甲基-1-苯基戊-1-烯-3-酮合成路线 （共 30 条）
反应条件
potassium phosphate; oxygen; AlO(OH); palladium in toluene T=110°C; P=760 Torr; 20 h;
参考文献
Kwon, Min Serk; Kim, Namdu; Seo, Seong Hyeok; Park, In Soo; Cheedrala, Ravi Kumar; Park, Jaiwook
Angewandte Chemie - International Edition, 2005 , vol. 44, # 42 p. 6913 - 6915
反应条件
Iron (III) nitrate nonahydrate; 2,2,6,6-tetramethyl-piperidine-N-oxyl; oxygen; sodium chloride in 1,2-dichloro-ethane T=25°C; P=760.051 Torr; 4 h;
参考文献
Ma, Shengming; Liu, Jinxian; Li, Suhua; Chen, Bo; Cheng, Jiajia; Kuang, Jinqiang; Liu, Yu; Wan, Baoqiang; Wang, Yuli; Ye, Juntao; Yu, Qiong; Yuan, Weiming; Yu, Shichao
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 6 p. 1005 - 1017
反应条件
1: isopropyllithium With indium(III) chloride in tetrahydrofuran; hexane T=-78°C; 0.5 h; 2: carbon monoxide; β-styryl bromide With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; hexane T=66°C; P=760 Torr; 3 h;
参考文献
Lee, Phil Ho; Lee, Sung Wook; Lee, Kooyeon
Organic Letters, 2003 , vol. 5, # 7 p. 1103 - 1106
反应条件
barium dihydroxide in ethanol 1 h; Heating;
参考文献
Sinisterra, J. V.; Garcia-Raso, A.; Cabello, J. A.; Marinas, J. M.
Synthesis, 1984 , # 6 p. 502 - 504
反应条件
[Rh(rac-BINAP)]BF4 in dichloromethane T=80°C; 1 h;
参考文献
Tanaka, Ken; Shoji, Takeaki; Hirano, Masao
European Journal of Organic Chemistry, 2007 , # 16 p. 2687 - 2699
反应条件
water; potassium carbonate in acetonitrile T=25°C; 18 h;
参考文献
Huang; Shi; Li
Synthesis, 1988 , # 12 p. 975 - 977
反应条件
in tetrahydrofuran T=-78°C; 1 h;
参考文献
Johnson, Carl R.; Dhanoa, Daljit S.
Journal of Organic Chemistry, 1987 , vol. 52, # 10 p. 1885 - 1888
反应条件
copper(l) iodide in tetrahydrofuran; diethyl ether T=20°C; Grignard reaction; 3 h;
参考文献
De Luca, Lidia; Giacomelli, Giampaolo; Porcheddu, Andrea
Organic Letters, 2001 , vol. 3, # 10 p. 1519 - 1521
反应条件
[Rh((R)-BINAP)]BF4 in dichloromethane T=25°C; 28 h;
参考文献
Tanaka, Ken; Shoji, Takeaki
Organic Letters, 2005 , vol. 7, # 16 p. 3561 - 3563
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; copper(l) iodide; methyllithium; diisobutylaluminium hydride in tetrahydrofuran; hexane T=-50°C; 2 h; Yield given. Yields of byproduct given;
参考文献
Tsuda, Tetsuo; Yoshida, Tsutomu; Kawamoto, Tadashi; Saegusa, Takeo
Journal of Organic Chemistry, 1987 , vol. 52, # 8 p. 1624 - 1627
