in benzene Ir complex (0.73 mmol) dissolved under Ar in C6H6 (8 ml); excess (CH2OMe)2 (0.7 ml) added; stirred (24 h, 80°C); evapd. (vac.); column chromd. (silica gel, hexane-Et2O, 10:1 3:1); Ir complex recrystd. from hexane-CH2Cl2 (3:2) at -20°C;
参考文献
Paneque, Margarita; Poveda, Manuel L.; Santos, Laura L.; Salazar, Veronica; Carmona, Ernesto
Chemical Communications, 2004 , # 16 p. 1838 - 1839
Koto, Shinkiti; Morishima, Naohiko; Kawahara, Reiko; Ishikawa, Katsuhiko; Zen, Shonosuke
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 4 p. 1092 - 1096
